Cost and energy saving process for the laboratory-scale production of chloroform-d

• Main Authors: Zaharani, Lia, Johan, Mohd Rafie, Khaligh, Nader Ghaffari
• Format: Article
• Published: American Chemical Society 2022
• Subjects: QD Chemistry
• Online Access: http://eprints.um.edu.my/40382/

Deuterochloroform (CDCl3), a commonly deuterated solvent in research and undergraduate laboratories and widely employed for nuclear magnetic resonance analyses, could be prepared using a more sustainable and efficient catalytic process. The synthesis includes a one-pot reaction of hexachloroacetone...