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Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method

This paper reports on the synthesis of copper selenide (CuSe) and tin selenide (SnSe) powders by high energy planetary ball milling, starting from elemental powders. Synthesis time and milling speed have been optimized to produce single phase CuSe and SnSe materials. The structural, compositional, m...

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Main Authors: Loh, Yen Nee, Talib, Zainal Abidin, Zainal, Zulkarnain, Liew, Josephine Ying Chyi
Format: Article
Published: Scientific.Net 2021
Online Access:http://psasir.upm.edu.my/id/eprint/95252/
https://www.scientific.net/SSP.317.152
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spelling my.upm.eprints.952522023-01-31T08:49:40Z http://psasir.upm.edu.my/id/eprint/95252/ Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method Loh, Yen Nee Talib, Zainal Abidin Zainal, Zulkarnain Liew, Josephine Ying Chyi This paper reports on the synthesis of copper selenide (CuSe) and tin selenide (SnSe) powders by high energy planetary ball milling, starting from elemental powders. Synthesis time and milling speed have been optimized to produce single phase CuSe and SnSe materials. The structural, compositional, morphological and optical properties of the synthesized samples have been analyzed by X-ray diffraction (XRD), transmission electron microscopy (TEM), Field Emission Scanning Electron Microscopy (FESEM) and UV-Vis. The low-temperature phase selection of the binary compound in this system is seen as a direct consequence of the thermodynamic facilitation, coupled with the capability of mechano-chemical synthesis to aid in overcoming kinetic constraints. Scientific.Net 2021 Article PeerReviewed Loh, Yen Nee and Talib, Zainal Abidin and Zainal, Zulkarnain and Liew, Josephine Ying Chyi (2021) Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method. Solid State Phenomena, 317. 152 - 156. ISSN 1012-0394; ESSN: 1662-9779 https://www.scientific.net/SSP.317.152 10.4028/www.scientific.net/SSP.317.152
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
description This paper reports on the synthesis of copper selenide (CuSe) and tin selenide (SnSe) powders by high energy planetary ball milling, starting from elemental powders. Synthesis time and milling speed have been optimized to produce single phase CuSe and SnSe materials. The structural, compositional, morphological and optical properties of the synthesized samples have been analyzed by X-ray diffraction (XRD), transmission electron microscopy (TEM), Field Emission Scanning Electron Microscopy (FESEM) and UV-Vis. The low-temperature phase selection of the binary compound in this system is seen as a direct consequence of the thermodynamic facilitation, coupled with the capability of mechano-chemical synthesis to aid in overcoming kinetic constraints.
format Article
author Loh, Yen Nee
Talib, Zainal Abidin
Zainal, Zulkarnain
Liew, Josephine Ying Chyi
spellingShingle Loh, Yen Nee
Talib, Zainal Abidin
Zainal, Zulkarnain
Liew, Josephine Ying Chyi
Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
author_facet Loh, Yen Nee
Talib, Zainal Abidin
Zainal, Zulkarnain
Liew, Josephine Ying Chyi
author_sort Loh, Yen Nee
title Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
title_short Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
title_full Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
title_fullStr Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
title_full_unstemmed Synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
title_sort synthesis and characterization of copper selenide and tin selenide powders by mechanical alloying method
publisher Scientific.Net
publishDate 2021
url http://psasir.upm.edu.my/id/eprint/95252/
https://www.scientific.net/SSP.317.152
_version_ 1756685772626329600
score 13.160551

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