Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Cit...
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my.upm.eprints.875362022-11-23T02:33:52Z http://psasir.upm.edu.my/id/eprint/87536/ Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Citrus hystrix leaves through a PHWE. A maximum Y% of 1.63% was successfully isolated at conditions involving 0.08% moisture content, 1 mm particle size, 1:0.2 ml/g solvent-to-sample ratio, 30 min extraction time, and 120°C extraction temperature. Moisture content and particle size were the main effects that significantly affect the %Y, while the extraction time and solvent-to-sample ratio exhibited a moderate effect on %Y, followed by extraction temperature that showed the least effect on %Y. A developed regression model has shown good correlation and adequacy on %Y. Based on the compositional analysis, neoisopulegol hydrate appears to be the main constituents of the oil obtained. Wiley 2020-09 Article PeerReviewed Abdul Halim, Noor Amirah and Zainal Abidin, Zurina and Siajam, Shamsul Izhar and Chong, Gun Hean and Harun, Mohd Razif (2020) Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design. Journal of Food Process Engineering, 43 (11). pp. 1-13. ISSN 1745-4530 https://onlinelibrary.wiley.com/doi/abs/10.1111/jfpe.13531 10.1111/jfpe.13531 |
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Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Citrus hystrix leaves through a PHWE. A maximum Y% of 1.63% was successfully isolated at conditions involving 0.08% moisture content, 1 mm particle size, 1:0.2 ml/g solvent-to-sample ratio, 30 min extraction time, and 120°C extraction temperature. Moisture content and particle size were the main effects that significantly affect the %Y, while the extraction time and solvent-to-sample ratio exhibited a moderate effect on %Y, followed by extraction temperature that showed the least effect on %Y. A developed regression model has shown good correlation and adequacy on %Y. Based on the compositional analysis, neoisopulegol hydrate appears to be the main constituents of the oil obtained. |
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Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif |
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Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
author_facet |
Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif |
author_sort |
Abdul Halim, Noor Amirah |
title |
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
title_short |
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
title_full |
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
title_fullStr |
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
title_full_unstemmed |
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design |
title_sort |
screening of factors influencing the yield of citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution v fractional factorial design |
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Wiley |
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2020 |
url |
http://psasir.upm.edu.my/id/eprint/87536/ https://onlinelibrary.wiley.com/doi/abs/10.1111/jfpe.13531 |
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1751538214442631168 |
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