Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina
Aluminum waste-can management in Malaysia has recently become a serious environmental and public health issue, particularly in metropolitan areas. This has prompted the need to valorize these waste-cans into value-added products using the most economical and environmentally friendly techniques. In t...
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my.utp.eprints.331102022-07-06T07:55:12Z Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina Bin Mokaizh, A.A. Shariffuddin, J.H. Baarimah, A.O. Al-Fakih, A. Mohamed, A. Baarimah, S.O. Al-Mekhlafi, A.-B.A. Alenezi, H. Olalere, O.A. Saeed, A.A.H. Aluminum waste-can management in Malaysia has recently become a serious environmental and public health issue, particularly in metropolitan areas. This has prompted the need to valorize these waste-cans into value-added products using the most economical and environmentally friendly techniques. In this study, the sol�gel technique was used to synthesize high-quality alumina from the aluminum waste-cans collected. From this method, the observed peaks of the synthesized alumina were identified as diaspore (α-AlO(OH)), boehmite (γ-AlO(OH)), aluminum oxide, or gamma-alumina (γ-Al2O3 ) crystalline structure and corundum. The morphological configuration, microstructure, and functional group properties of the synthesized alumina were evaluated. All the synthesized alumina exhibited a non-spherical shape and appeared to have hexagonal-like shape particles. Moreover, the XRD patterns of the synthesized alumina AL-6-30 and AL-12-30 exhibited a small angle (1�10� ) with no XRD peak, which indicated a mesoporous pore structure with no long-range order. The overall results of γ-alumina synthesized from the aluminum waste-cans showed an optimal condition in producing a highly structured γ-alumina with excellent surface-area characteristics. The synthesized alumina exhibited stronger and highly crystalline functional characteristics almost comparable with the commercially available brands on the market. © 2022 by the authors. Licensee MDPI, Basel, Switzerland. MDPI 2022 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85129279512&doi=10.3390%2fma15093046&partnerID=40&md5=f3d51b5e206243f6ea14c0e4c96ee009 Bin Mokaizh, A.A. and Shariffuddin, J.H. and Baarimah, A.O. and Al-Fakih, A. and Mohamed, A. and Baarimah, S.O. and Al-Mekhlafi, A.-B.A. and Alenezi, H. and Olalere, O.A. and Saeed, A.A.H. (2022) Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina. Materials, 15 (9). http://eprints.utp.edu.my/33110/ |
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Aluminum waste-can management in Malaysia has recently become a serious environmental and public health issue, particularly in metropolitan areas. This has prompted the need to valorize these waste-cans into value-added products using the most economical and environmentally friendly techniques. In this study, the sol�gel technique was used to synthesize high-quality alumina from the aluminum waste-cans collected. From this method, the observed peaks of the synthesized alumina were identified as diaspore (α-AlO(OH)), boehmite (γ-AlO(OH)), aluminum oxide, or gamma-alumina (γ-Al2O3 ) crystalline structure and corundum. The morphological configuration, microstructure, and functional group properties of the synthesized alumina were evaluated. All the synthesized alumina exhibited a non-spherical shape and appeared to have hexagonal-like shape particles. Moreover, the XRD patterns of the synthesized alumina AL-6-30 and AL-12-30 exhibited a small angle (1�10� ) with no XRD peak, which indicated a mesoporous pore structure with no long-range order. The overall results of γ-alumina synthesized from the aluminum waste-cans showed an optimal condition in producing a highly structured γ-alumina with excellent surface-area characteristics. The synthesized alumina exhibited stronger and highly crystalline functional characteristics almost comparable with the commercially available brands on the market. © 2022 by the authors. Licensee MDPI, Basel, Switzerland. |
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Article |
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Bin Mokaizh, A.A. Shariffuddin, J.H. Baarimah, A.O. Al-Fakih, A. Mohamed, A. Baarimah, S.O. Al-Mekhlafi, A.-B.A. Alenezi, H. Olalere, O.A. Saeed, A.A.H. |
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Bin Mokaizh, A.A. Shariffuddin, J.H. Baarimah, A.O. Al-Fakih, A. Mohamed, A. Baarimah, S.O. Al-Mekhlafi, A.-B.A. Alenezi, H. Olalere, O.A. Saeed, A.A.H. Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
author_facet |
Bin Mokaizh, A.A. Shariffuddin, J.H. Baarimah, A.O. Al-Fakih, A. Mohamed, A. Baarimah, S.O. Al-Mekhlafi, A.-B.A. Alenezi, H. Olalere, O.A. Saeed, A.A.H. |
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Bin Mokaizh, A.A. |
title |
Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
title_short |
Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
title_full |
Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
title_fullStr |
Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
title_full_unstemmed |
Elucidating the Effects of Reaction Time on the Physicochemical Characterization of Valorized Synthesized Alumina |
title_sort |
elucidating the effects of reaction time on the physicochemical characterization of valorized synthesized alumina |
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MDPI |
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2022 |
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https://www.scopus.com/inward/record.uri?eid=2-s2.0-85129279512&doi=10.3390%2fma15093046&partnerID=40&md5=f3d51b5e206243f6ea14c0e4c96ee009 http://eprints.utp.edu.my/33110/ |
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13.159267 |