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Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate

The title compound has been synthesized by grinding in an agate mortar. Its structure was characterized by TGA-DSC studies and single-crystal X-ray diffraction. This compound crystallize in the monoclinic system with space group C2/c, Z = 4, and unit cell parameters a = 16.109(2) Å, b = 5.748(7) Å,...

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Main Authors: Chacon, Cecilia, Bruno Colmenarez, Julia, Jamalis, Joazaizulfazli, Delgado, Gerzon E.
Format: Article
Language:English
Published: Vasile Alecsandri Univ Bacau 2017
Subjects:
QD Chemistry
Online Access:http://eprints.utm.my/id/eprint/77537/1/JoazaizulfazliJamalis2017_SynthesisThermalStudiesandCrystalStructure.pdf
http://eprints.utm.my/id/eprint/77537/
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spelling my.utm.775372020-12-01T07:56:40Z http://eprints.utm.my/id/eprint/77537/ Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate Chacon, Cecilia Bruno Colmenarez, Julia Jamalis, Joazaizulfazli Delgado, Gerzon E. QD Chemistry The title compound has been synthesized by grinding in an agate mortar. Its structure was characterized by TGA-DSC studies and single-crystal X-ray diffraction. This compound crystallize in the monoclinic system with space group C2/c, Z = 4, and unit cell parameters a = 16.109(2) Å, b = 5.748(7) Å, c = 20.580(3) Å, β = 107.36(1)°. The salt, C2HO4 -.C5H7N+.0.5 H2O, is an ionic ensemble assisted by hydrogen bonds established between 4-aminopyridinium cations, oxalate anions and water molecules. The three components thus construct a supramolecular assembly with a three-dimensional hydrogen bonded framework. Vasile Alecsandri Univ Bacau 2017 Article PeerReviewed application/pdf en http://eprints.utm.my/id/eprint/77537/1/JoazaizulfazliJamalis2017_SynthesisThermalStudiesandCrystalStructure.pdf Chacon, Cecilia and Bruno Colmenarez, Julia and Jamalis, Joazaizulfazli and Delgado, Gerzon E. (2017) Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate. Scientific Study and Research: Chemistry and Chemical Engineering, Biotechnology, Food Industry, 18 (2). pp. 111-119. ISSN 1582-540X
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Chacon, Cecilia
Bruno Colmenarez, Julia
Jamalis, Joazaizulfazli
Delgado, Gerzon E.
Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
description The title compound has been synthesized by grinding in an agate mortar. Its structure was characterized by TGA-DSC studies and single-crystal X-ray diffraction. This compound crystallize in the monoclinic system with space group C2/c, Z = 4, and unit cell parameters a = 16.109(2) Å, b = 5.748(7) Å, c = 20.580(3) Å, β = 107.36(1)°. The salt, C2HO4 -.C5H7N+.0.5 H2O, is an ionic ensemble assisted by hydrogen bonds established between 4-aminopyridinium cations, oxalate anions and water molecules. The three components thus construct a supramolecular assembly with a three-dimensional hydrogen bonded framework.
format Article
author Chacon, Cecilia
Bruno Colmenarez, Julia
Jamalis, Joazaizulfazli
Delgado, Gerzon E.
author_facet Chacon, Cecilia
Bruno Colmenarez, Julia
Jamalis, Joazaizulfazli
Delgado, Gerzon E.
author_sort Chacon, Cecilia
title Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
title_short Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
title_full Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
title_fullStr Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
title_full_unstemmed Synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
title_sort synthesis, thermal studies and crystal structure of 4-aminopyridinium semi-oxalate hemihydrate
publisher Vasile Alecsandri Univ Bacau
publishDate 2017
url http://eprints.utm.my/id/eprint/77537/1/JoazaizulfazliJamalis2017_SynthesisThermalStudiesandCrystalStructure.pdf
http://eprints.utm.my/id/eprint/77537/
_version_ 1685578928495788032
score 13.211869

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