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Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques

A new elastomer was successfully materialized from sunflower oil (a vegetable oil). The reaction was confirmed by Fourier Transform Infrared (FTIR) and Fourier Transform Nuclear Magnetic Resonance (FTNMR) methods. FTIR analysis indicated that amine functional groups appear at 3325 cm-1 representing...

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Main Authors: Purbaya, Mili, Mohd. Nor, Hussin, Suwardin, Didin
格式: Article
出版: Wiley-VCH Verlag 2015
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TP Chemical technology
在線閱讀:http://eprints.utm.my/id/eprint/58867/
http://dx.doi.org/10.1002/masy.201550322
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spelling my.utm.588672021-12-16T03:01:19Z http://eprints.utm.my/id/eprint/58867/ Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques Purbaya, Mili Mohd. Nor, Hussin Suwardin, Didin TP Chemical technology A new elastomer was successfully materialized from sunflower oil (a vegetable oil). The reaction was confirmed by Fourier Transform Infrared (FTIR) and Fourier Transform Nuclear Magnetic Resonance (FTNMR) methods. FTIR analysis indicated that amine functional groups appear at 3325 cm-1 representing N-H stretching of primary and secondary amines and at 1645 cm-1 representing N-H deformation of primary amines. The hydrogen bonding was confirmed with the appearance a broad peak in the region 2500-3800 cm-1. FTNMR analysis also show the appearance amine functional groups at peak 5.4 ppm in 1H NMR representing proton in amine functional groups and peaks at 151 ppm and 156.6 ppm in 13C NMR representing carbon in amine functional groups. Wiley-VCH Verlag 2015 Article PeerReviewed Purbaya, Mili and Mohd. Nor, Hussin and Suwardin, Didin (2015) Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques. Macromolecular Symposia, 353 (1). pp. 161-167. ISSN 1022-1360 http://dx.doi.org/10.1002/masy.201550322 DOI: 10.1002/masy.201550322
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
topic TP Chemical technology
spellingShingle TP Chemical technology
Purbaya, Mili
Mohd. Nor, Hussin
Suwardin, Didin
Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
description A new elastomer was successfully materialized from sunflower oil (a vegetable oil). The reaction was confirmed by Fourier Transform Infrared (FTIR) and Fourier Transform Nuclear Magnetic Resonance (FTNMR) methods. FTIR analysis indicated that amine functional groups appear at 3325 cm-1 representing N-H stretching of primary and secondary amines and at 1645 cm-1 representing N-H deformation of primary amines. The hydrogen bonding was confirmed with the appearance a broad peak in the region 2500-3800 cm-1. FTNMR analysis also show the appearance amine functional groups at peak 5.4 ppm in 1H NMR representing proton in amine functional groups and peaks at 151 ppm and 156.6 ppm in 13C NMR representing carbon in amine functional groups.
format Article
author Purbaya, Mili
Mohd. Nor, Hussin
Suwardin, Didin
author_facet Purbaya, Mili
Mohd. Nor, Hussin
Suwardin, Didin
author_sort Purbaya, Mili
title Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
title_short Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
title_full Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
title_fullStr Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
title_full_unstemmed Synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
title_sort synthesis of sunflower oil based elastomer and its characterization by using spectroscopic techniques
publisher Wiley-VCH Verlag
publishDate 2015
url http://eprints.utm.my/id/eprint/58867/
http://dx.doi.org/10.1002/masy.201550322
_version_ 1720436893310517248
score 13.250246

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