Microwave irradiation technique for synthesis of zeolite A
Synthesization of Zeolite A from colloidal silica was performed by means of microwave irradiation technique under different conditions and was compared with hydrothermal technique. The molar composition at 1 Al203: 1.96 SiO2: 3.165 Na2O: 128 H2O. X-Ray Diffraction (XRD) and Scanning Electron Microsc...
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Main Authors: | , , , |
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Format: | Conference or Workshop Item |
Language: | English |
Published: |
2007
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Subjects: | |
Online Access: | http://eprints.utm.my/id/eprint/5697/1/H.M.Razif2007_MicrowaveIrradiationTechniqueForSynthesisOfZeoliteA.pdf http://eprints.utm.my/id/eprint/5697/ |
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Summary: | Synthesization of Zeolite A from colloidal silica was performed by means of microwave irradiation technique under different conditions and was compared with hydrothermal technique. The molar composition at 1 Al203: 1.96 SiO2: 3.165 Na2O: 128 H2O. X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM) were used to characterize zeolite A. XRD results for all samples demonstrated a typical diffraction peak of zeolite A. SEM images show almost no-different in crystal size of zeolite A synthesized by microwave irradiation and hydrothermal technique. Thus, we concluded that crystallization of zeolite A has occurred rapidly by microwave irradiation. Microwave technique is a time and energy saving due to crystallization time and higher heating rate as compared to hydrothermal technique. |
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