Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel
Carbon-based catalysts were reported to hold advantages such as being cost-effective, eco-friendly while having good stability and high selectivity in catalytic processes. Optimization of sulfonated sago pith waste (s-SPW) catalyst as a starch-rich biomass-derived solid acid catalyst for conversion...
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Italian Association of Chemical Engineering - AIDIC
2023
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Online Access: | http://eprints.utm.my/105993/1/ZakiYamaniZakaria2023_OptimizationofSulfonatedSagoPithWasteCatalyst.pdf http://eprints.utm.my/105993/ http://dx.doi.org/10.3303/CET23106138 |
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my.utm.1059932024-05-31T02:48:25Z http://eprints.utm.my/105993/ Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel Tan, Wan Ting Jusoh, Mazura Zakaria, Zaki Yamani TP Chemical technology Carbon-based catalysts were reported to hold advantages such as being cost-effective, eco-friendly while having good stability and high selectivity in catalytic processes. Optimization of sulfonated sago pith waste (s-SPW) catalyst as a starch-rich biomass-derived solid acid catalyst for conversion of palm fatty acid distillate (PFAD) feedstock to biodiesel product was performed in this study. Synthesis condition of s-SPW catalyst was optimized through the design of experiment (DOE) optimization by employing Response Surface Methodology (RSM) using Statistica Software V10.0. Four independent variables for the synthesis of s-SPW catalyst, including carbonization temperature, carbonization time, sulfonation temperature and sulfonation time were studied for the optimization work with the response of biodiesel yield. DOE was carried out by utilizing Central Composite Design (CCD) of 4 factors with 26 runs. The optimum synthesis condition of s-SPW catalyst was found at a carbonization temperature of 338.49 °C, carbonization time of 69.44 min, sulfonation temperature of 156.32 °C and sulfonation time of 7.13 min with a biodiesel yield of 69.51 %. Conversion of PFAD with s-SPW catalyst is a promising, greener and cost-effective synthetic route for biodiesel production. Italian Association of Chemical Engineering - AIDIC 2023 Article PeerReviewed application/pdf en http://eprints.utm.my/105993/1/ZakiYamaniZakaria2023_OptimizationofSulfonatedSagoPithWasteCatalyst.pdf Tan, Wan Ting and Jusoh, Mazura and Zakaria, Zaki Yamani (2023) Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel. Chemical Engineering Transactions, 106 (NA). pp. 823-828. ISSN 2283-9216 http://dx.doi.org/10.3303/CET23106138 DOI : 10.3303/CET23106138 |
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TP Chemical technology Tan, Wan Ting Jusoh, Mazura Zakaria, Zaki Yamani Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
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Carbon-based catalysts were reported to hold advantages such as being cost-effective, eco-friendly while having good stability and high selectivity in catalytic processes. Optimization of sulfonated sago pith waste (s-SPW) catalyst as a starch-rich biomass-derived solid acid catalyst for conversion of palm fatty acid distillate (PFAD) feedstock to biodiesel product was performed in this study. Synthesis condition of s-SPW catalyst was optimized through the design of experiment (DOE) optimization by employing Response Surface Methodology (RSM) using Statistica Software V10.0. Four independent variables for the synthesis of s-SPW catalyst, including carbonization temperature, carbonization time, sulfonation temperature and sulfonation time were studied for the optimization work with the response of biodiesel yield. DOE was carried out by utilizing Central Composite Design (CCD) of 4 factors with 26 runs. The optimum synthesis condition of s-SPW catalyst was found at a carbonization temperature of 338.49 °C, carbonization time of 69.44 min, sulfonation temperature of 156.32 °C and sulfonation time of 7.13 min with a biodiesel yield of 69.51 %. Conversion of PFAD with s-SPW catalyst is a promising, greener and cost-effective synthetic route for biodiesel production. |
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Article |
author |
Tan, Wan Ting Jusoh, Mazura Zakaria, Zaki Yamani |
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Tan, Wan Ting Jusoh, Mazura Zakaria, Zaki Yamani |
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Tan, Wan Ting |
title |
Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
title_short |
Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
title_full |
Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
title_fullStr |
Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
title_full_unstemmed |
Optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
title_sort |
optimization of sulfonated sago pith waste catalyst for conversion of palm fatty acid distillate to biodiesel |
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Italian Association of Chemical Engineering - AIDIC |
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2023 |
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http://eprints.utm.my/105993/1/ZakiYamaniZakaria2023_OptimizationofSulfonatedSagoPithWasteCatalyst.pdf http://eprints.utm.my/105993/ http://dx.doi.org/10.3303/CET23106138 |
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13.160551 |