FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method

Composites material were developed to acquire the desired material properties for biomedical applications in the recovery of defect bone by using Mg-doped HA/SA. Hydroxyapatite (HA) is the major constituent and essential component in bone and teeth. The stability of Mg-doped HA/SA is influenced by s...

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Main Authors: Kanasan, Nanthini, Adzila, S., Rahman, H. A., Bano, Nazia, Panerselvan, G.
格式: Article
語言:English
出版: Trans Tech Publications 2018
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spelling my.uthm.eprints.45442021-12-07T06:34:23Z http://eprints.uthm.edu.my/4544/ FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method Kanasan, Nanthini Adzila, S. Rahman, H. A. Bano, Nazia Panerselvan, G. TA401-492 Materials of engineering and construction. Mechanics of materials Composites material were developed to acquire the desired material properties for biomedical applications in the recovery of defect bone by using Mg-doped HA/SA. Hydroxyapatite (HA) is the major constituent and essential component in bone and teeth. The stability of Mg-doped HA/SA is influenced by starting precursor powders, preparation condition and method of preparing the samples for implant materials. The precipitation method was employed to prepare Mg-doped HA/SA powders by varying the composition of Mg at temperature 1300°C. The influence of Mg-doped HA/SA on phase composition, chemical structure and a functional group at various weight percentages (0.5wt%-1.5wt %) were accomplished through X-ray diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR) analyses. Based on the XRD and FTIR analyses, there is the presence of different peaks intensity and adsorption bands which indicates the shifted of peaks due to the doping process and a chemical interaction were observed between the inorganic and organic phase. Furthermore, the transformation of β-TCP due to increase in sintering temperatures are caused by the presence of magnesium ions. The OHstretching bands of HA/SA are traced by FTIR that identified the decomposition of Mg-doped HA/SA. Trans Tech Publications 2018 Article PeerReviewed text en http://eprints.uthm.edu.my/4544/1/AJ%202018%20%28788%29%20FTIR%20and%20XRD%20evaluation%20of%20magnesium%20doped%20hydroxyapatitesodium%20alginate%20powder%20by%20precipitation%20method.pdf Kanasan, Nanthini and Adzila, S. and Rahman, H. A. and Bano, Nazia and Panerselvan, G. (2018) FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method. Key Engineering Materials, 791. pp. 45-49. ISSN 1662-9795
institution Universiti Tun Hussein Onn Malaysia
building UTHM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Tun Hussein Onn Malaysia
content_source UTHM Institutional Repository
url_provider http://eprints.uthm.edu.my/
language English
topic TA401-492 Materials of engineering and construction. Mechanics of materials
spellingShingle TA401-492 Materials of engineering and construction. Mechanics of materials
Kanasan, Nanthini
Adzila, S.
Rahman, H. A.
Bano, Nazia
Panerselvan, G.
FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
description Composites material were developed to acquire the desired material properties for biomedical applications in the recovery of defect bone by using Mg-doped HA/SA. Hydroxyapatite (HA) is the major constituent and essential component in bone and teeth. The stability of Mg-doped HA/SA is influenced by starting precursor powders, preparation condition and method of preparing the samples for implant materials. The precipitation method was employed to prepare Mg-doped HA/SA powders by varying the composition of Mg at temperature 1300°C. The influence of Mg-doped HA/SA on phase composition, chemical structure and a functional group at various weight percentages (0.5wt%-1.5wt %) were accomplished through X-ray diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR) analyses. Based on the XRD and FTIR analyses, there is the presence of different peaks intensity and adsorption bands which indicates the shifted of peaks due to the doping process and a chemical interaction were observed between the inorganic and organic phase. Furthermore, the transformation of β-TCP due to increase in sintering temperatures are caused by the presence of magnesium ions. The OHstretching bands of HA/SA are traced by FTIR that identified the decomposition of Mg-doped HA/SA.
format Article
author Kanasan, Nanthini
Adzila, S.
Rahman, H. A.
Bano, Nazia
Panerselvan, G.
author_facet Kanasan, Nanthini
Adzila, S.
Rahman, H. A.
Bano, Nazia
Panerselvan, G.
author_sort Kanasan, Nanthini
title FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
title_short FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
title_full FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
title_fullStr FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
title_full_unstemmed FTIR and XRD evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
title_sort ftir and xrd evaluation of magnesium doped hydroxyapatitesodium alginate powder by precipitation method
publisher Trans Tech Publications
publishDate 2018
url http://eprints.uthm.edu.my/4544/1/AJ%202018%20%28788%29%20FTIR%20and%20XRD%20evaluation%20of%20magnesium%20doped%20hydroxyapatitesodium%20alginate%20powder%20by%20precipitation%20method.pdf
http://eprints.uthm.edu.my/4544/
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