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Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method

Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine...

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Main Author: Al-Amani, Umar
Format: Conference or Workshop Item
Language:English
Published: 2009
Subjects:
T Technology (General)
Online Access:http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf
http://eprints.utem.edu.my/id/eprint/9785/
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spelling my.utem.eprints.97852015-05-28T04:06:35Z http://eprints.utem.edu.my/id/eprint/9785/ Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method Al-Amani, Umar T Technology (General) Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine the formation of Bi4Ti3O12. Pure Bi4Ti3O12 powder was successfully formed with Ti addition after calcination at 800oC for 3 h. The average crystallite sizes produced were 77.9 nm, 63.6 nm and 51.8 nm with mol ratio of 4:3.1, 4:3.4 and 4:3.6, respectively. The results obtained infer that the relative amount of Ti was identified as limiting reagent in the combustion reaction and was also considered as key factor to achieve single-phase Bi4Ti3O12 2009 Conference or Workshop Item PeerReviewed application/pdf en http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf Al-Amani, Umar (2009) Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method. In: 4th International Conference on Recent Advances in Materials, Minerals, Environment and 2nd Asian Symposium on materials and Processing (RAMM & ASMP), 1-3 Jun 2009, Bayview Beach Resort, Batu Ferringi, Penang, Malaysia.
institution Universiti Teknikal Malaysia Melaka
building UTEM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknikal Malaysia Melaka
content_source UTEM Institutional Repository
url_provider http://eprints.utem.edu.my/
language English
topic T Technology (General)
spellingShingle T Technology (General)
Al-Amani, Umar
Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
description Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine the formation of Bi4Ti3O12. Pure Bi4Ti3O12 powder was successfully formed with Ti addition after calcination at 800oC for 3 h. The average crystallite sizes produced were 77.9 nm, 63.6 nm and 51.8 nm with mol ratio of 4:3.1, 4:3.4 and 4:3.6, respectively. The results obtained infer that the relative amount of Ti was identified as limiting reagent in the combustion reaction and was also considered as key factor to achieve single-phase Bi4Ti3O12
format Conference or Workshop Item
author Al-Amani, Umar
author_facet Al-Amani, Umar
author_sort Al-Amani, Umar
title Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
title_short Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
title_full Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
title_fullStr Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
title_full_unstemmed Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
title_sort effect of bi and ti additions on the phase formation of bi4ti3o12 using fuel-free combustion method
publishDate 2009
url http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf
http://eprints.utem.edu.my/id/eprint/9785/
_version_ 1665905407739035648
score 13.18916

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