Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method
Nanostructured LiMnPO4 cathode materials were successfully achieved by sol–gel route with the aid of oxalic acid and nitric acid. The effects of sintering temperatures on structural properties especially strain and crystallite size were analysed. The structural crystallinity and average particle siz...
Saved in:
Main Authors: | , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Springer
2016
|
Subjects: | |
Online Access: | http://eprints.utem.edu.my/id/eprint/17019/2/rajammal2016.pdf http://eprints.utem.edu.my/id/eprint/17019/ http://link.springer.com/article/10.1007/s10971-016-4111-3 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
id |
my.utem.eprints.17019 |
---|---|
record_format |
eprints |
spelling |
my.utem.eprints.170192021-09-07T22:44:08Z http://eprints.utem.edu.my/id/eprint/17019/ Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method K., Rajammal Sivakumar, Dhar Malingam Navaneethan, Duraisamy K., Ramesh S., Ramesh T Technology (General) Nanostructured LiMnPO4 cathode materials were successfully achieved by sol–gel route with the aid of oxalic acid and nitric acid. The effects of sintering temperatures on structural properties especially strain and crystallite size were analysed. The structural crystallinity and average particle sizes (42–77 nm) of LiMnPO4 are significantly varied with respect to calcination temperatures. LiMnPO4 obtained at 700 �C exhibits superior electrochemical performance among the samples. It delivered initial discharge capacity of 103.4 mAh g-1 at 0.05 C. These results revealed that the sol–gel technique could be favourable method to produce nanosized LiMnPO4 as a cathode material for lithium ion batteries via optimizing calcination temperatures. Springer 2016 Article PeerReviewed text en http://eprints.utem.edu.my/id/eprint/17019/2/rajammal2016.pdf K., Rajammal and Sivakumar, Dhar Malingam and Navaneethan, Duraisamy and K., Ramesh and S., Ramesh (2016) Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method. Journal Of Sol-Gel Science And Technology, 79. pp. 1-9. ISSN 0928-0707 http://link.springer.com/article/10.1007/s10971-016-4111-3 10.1007/s10971-016-4111-3 |
institution |
Universiti Teknikal Malaysia Melaka |
building |
UTEM Library |
collection |
Institutional Repository |
continent |
Asia |
country |
Malaysia |
content_provider |
Universiti Teknikal Malaysia Melaka |
content_source |
UTEM Institutional Repository |
url_provider |
http://eprints.utem.edu.my/ |
language |
English |
topic |
T Technology (General) |
spellingShingle |
T Technology (General) K., Rajammal Sivakumar, Dhar Malingam Navaneethan, Duraisamy K., Ramesh S., Ramesh Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
description |
Nanostructured LiMnPO4 cathode materials were successfully achieved by sol–gel route with the aid of oxalic acid and nitric acid. The effects of sintering temperatures on structural properties especially strain and crystallite size were analysed. The structural crystallinity and average particle sizes (42–77 nm) of LiMnPO4 are significantly varied with respect to calcination temperatures. LiMnPO4 obtained at 700 �C exhibits superior
electrochemical performance among the samples. It delivered
initial discharge capacity of 103.4 mAh g-1 at 0.05 C. These results revealed that the sol–gel technique could be
favourable method to produce nanosized LiMnPO4 as a cathode material for lithium ion batteries via optimizing calcination temperatures. |
format |
Article |
author |
K., Rajammal Sivakumar, Dhar Malingam Navaneethan, Duraisamy K., Ramesh S., Ramesh |
author_facet |
K., Rajammal Sivakumar, Dhar Malingam Navaneethan, Duraisamy K., Ramesh S., Ramesh |
author_sort |
K., Rajammal |
title |
Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
title_short |
Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
title_full |
Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
title_fullStr |
Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
title_full_unstemmed |
Effect Of Sintering Temperature On Structural Properties Of LiMnPO4 Cathode Materials Obtained By Sol–Gel Method |
title_sort |
effect of sintering temperature on structural properties of limnpo4 cathode materials obtained by sol–gel method |
publisher |
Springer |
publishDate |
2016 |
url |
http://eprints.utem.edu.my/id/eprint/17019/2/rajammal2016.pdf http://eprints.utem.edu.my/id/eprint/17019/ http://link.springer.com/article/10.1007/s10971-016-4111-3 |
_version_ |
1710679412469399552 |
score |
13.160551 |