Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics
Bismuth titanate, Bi4Ti3O12 was prepared at different hydrolysis temperature and characterized with XRD, Rietveld analysis, TG-DTA, FESEM and TEM. The results indicated that the pure bismuth titanate was obtained after combustion at lower temperature of about 260oC. Interestingly, no calcination ste...
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my.utem.eprints.100682015-05-28T04:08:50Z http://eprints.utem.edu.my/id/eprint/10068/ Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics Al-Amani, Umar T Technology (General) Bismuth titanate, Bi4Ti3O12 was prepared at different hydrolysis temperature and characterized with XRD, Rietveld analysis, TG-DTA, FESEM and TEM. The results indicated that the pure bismuth titanate was obtained after combustion at lower temperature of about 260oC. Interestingly, no calcination step involved to obtain bismuth-structured layered. The effect of hydrolysis temperature at 40, 50 and 60oC on phase formation, lattice parameter, crystallite size, thermal behavior as well as grain morphologies was investigated. Universiti Putra Malaysia 2010 Article PeerReviewed application/pdf en http://eprints.utem.edu.my/id/eprint/10068/1/MJM_Vol_6_2010.pdf Al-Amani, Umar (2010) Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics. Malaysian Journal of Microscopy. pp. 69-74. ISSN 1823 7010 |
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T Technology (General) Al-Amani, Umar Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
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Bismuth titanate, Bi4Ti3O12 was prepared at different hydrolysis temperature and characterized with XRD, Rietveld analysis, TG-DTA, FESEM and TEM. The results indicated that the pure bismuth titanate was obtained after combustion at lower temperature of about 260oC. Interestingly, no calcination step involved to obtain bismuth-structured layered. The effect of hydrolysis temperature at 40, 50 and 60oC on phase formation, lattice parameter, crystallite size, thermal behavior as well as grain morphologies was investigated. |
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Article |
author |
Al-Amani, Umar |
author_facet |
Al-Amani, Umar |
author_sort |
Al-Amani, Umar |
title |
Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
title_short |
Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
title_full |
Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
title_fullStr |
Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
title_full_unstemmed |
Low-temperature combustion synthesis of Bi4Ti3O12 plate-like structure and some of its characteristics |
title_sort |
low-temperature combustion synthesis of bi4ti3o12 plate-like structure and some of its characteristics |
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Universiti Putra Malaysia |
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2010 |
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http://eprints.utem.edu.my/id/eprint/10068/1/MJM_Vol_6_2010.pdf http://eprints.utem.edu.my/id/eprint/10068/ |
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