Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation
In this study, synthesis and characterization of chitosan/maghemite (Cs/Fe2O3) composites thin film has been described. Its properties were characterized using Fourier transform infrared spectroscopy (FTIR), atomic force microscopy (AFM) and ultraviolet-visible spectroscopy (UV-Vis). FTIR confirmed...
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Multidisciplinary Digital Publishing Institute
2020
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Online Access: | http://psasir.upm.edu.my/id/eprint/86880/1/Nanostructured%20chitosan.pdf http://psasir.upm.edu.my/id/eprint/86880/ https://www.mdpi.com/2073-4360/12/7/1497 |
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my.upm.eprints.868802021-12-30T07:28:55Z http://psasir.upm.edu.my/id/eprint/86880/ Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation Muhamad Fauzi, Nurul Illya Yap, Wing Fen Sheh Omar, Nur Alia Saleviter, Silvan Mohd Daniyal, Wan Mohd Ebtisyam Mustaqim Hashim, Hazwani Suhaila Mohd Nasrullah In this study, synthesis and characterization of chitosan/maghemite (Cs/Fe2O3) composites thin film has been described. Its properties were characterized using Fourier transform infrared spectroscopy (FTIR), atomic force microscopy (AFM) and ultraviolet-visible spectroscopy (UV-Vis). FTIR confirmed the existence of Fe–O bond, C–N bond, C–C bond, C–O bond, O=C=O bond and O–H bond in Cs/Fe2O3 thin film. The surface morphology of the thin film indicated the relatively smooth and homogenous thin film, and also confirmed the interaction of Fe2O3 with the chitosan. Next, the UV-Vis result showed high absorbance value with an optical band gap of 4.013 eV. The incorporation of this Cs/Fe2O3 thin film with an optical-based method, i.e., surface plasmon resonance spectroscopy showed positive response where mercury ion (Hg2+) can be detected down to 0.01 ppm (49.9 nM). These results validate the potential of Cs/Fe2O3 thin film for optical sensing applications in Hg2+ detection. Multidisciplinary Digital Publishing Institute 2020-07-04 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/86880/1/Nanostructured%20chitosan.pdf Muhamad Fauzi, Nurul Illya and Yap, Wing Fen and Sheh Omar, Nur Alia and Saleviter, Silvan and Mohd Daniyal, Wan Mohd Ebtisyam Mustaqim and Hashim, Hazwani Suhaila and Mohd Nasrullah (2020) Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation. Polymers, 12 (7). pp. 1-13. ISSN 2073-4360 https://www.mdpi.com/2073-4360/12/7/1497 10.3390/polym12071497 |
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In this study, synthesis and characterization of chitosan/maghemite (Cs/Fe2O3) composites thin film has been described. Its properties were characterized using Fourier transform infrared spectroscopy (FTIR), atomic force microscopy (AFM) and ultraviolet-visible spectroscopy (UV-Vis). FTIR confirmed the existence of Fe–O bond, C–N bond, C–C bond, C–O bond, O=C=O bond and O–H bond in Cs/Fe2O3 thin film. The surface morphology of the thin film indicated the relatively smooth and homogenous thin film, and also confirmed the interaction of Fe2O3 with the chitosan. Next, the UV-Vis result showed high absorbance value with an optical band gap of 4.013 eV. The incorporation of this Cs/Fe2O3 thin film with an optical-based method, i.e., surface plasmon resonance spectroscopy showed positive response where mercury ion (Hg2+) can be detected down to 0.01 ppm (49.9 nM). These results validate the potential of Cs/Fe2O3 thin film for optical sensing applications in Hg2+ detection. |
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Article |
author |
Muhamad Fauzi, Nurul Illya Yap, Wing Fen Sheh Omar, Nur Alia Saleviter, Silvan Mohd Daniyal, Wan Mohd Ebtisyam Mustaqim Hashim, Hazwani Suhaila Mohd Nasrullah |
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Muhamad Fauzi, Nurul Illya Yap, Wing Fen Sheh Omar, Nur Alia Saleviter, Silvan Mohd Daniyal, Wan Mohd Ebtisyam Mustaqim Hashim, Hazwani Suhaila Mohd Nasrullah Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
author_facet |
Muhamad Fauzi, Nurul Illya Yap, Wing Fen Sheh Omar, Nur Alia Saleviter, Silvan Mohd Daniyal, Wan Mohd Ebtisyam Mustaqim Hashim, Hazwani Suhaila Mohd Nasrullah |
author_sort |
Muhamad Fauzi, Nurul Illya |
title |
Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
title_short |
Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
title_full |
Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
title_fullStr |
Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
title_full_unstemmed |
Nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
title_sort |
nanostructured chitosan/maghemite composites thin film for potential optical detection of mercury ion by surface plasmon resonance investigation |
publisher |
Multidisciplinary Digital Publishing Institute |
publishDate |
2020 |
url |
http://psasir.upm.edu.my/id/eprint/86880/1/Nanostructured%20chitosan.pdf http://psasir.upm.edu.my/id/eprint/86880/ https://www.mdpi.com/2073-4360/12/7/1497 |
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