Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6...
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Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry
2017
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| Online Access: | http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf http://psasir.upm.edu.my/id/eprint/61263/ https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article |
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my.upm.eprints.612632022-03-04T07:52:21Z http://psasir.upm.edu.my/id/eprint/61263/ Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice. Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry 2017 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf M. Osman, Uwaisulqarni and Mohamed Tahir, Mohamed Ibrahim and Crouse, Karen Anne and Ravoof, Thahira Begum S. A. (2017) Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate. X-ray Structure Analysis Online, 33 (9). 57 - 58. ISSN 1883-3578 (Unpublished) https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article 10.2116/xraystruct.33.57 |
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The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice. |
| format |
Article |
| author |
M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. |
| spellingShingle |
M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| author_facet |
M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. |
| author_sort |
M. Osman, Uwaisulqarni |
| title |
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_short |
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_full |
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_fullStr |
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_full_unstemmed |
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_sort |
crystal structure of methyl-n′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| publisher |
Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry |
| publishDate |
2017 |
| url |
http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf http://psasir.upm.edu.my/id/eprint/61263/ https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article |
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13.18916 |