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Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids

A new method is developed to determine veterinary antibiotics and hormone in solid environmental samples by high performance liquid chromatography combined with tandem mass spectrometry (HPLC-MS/MS) using isotope dilution and internal standard quantitation techniques. This method has been developed...

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Main Authors: Zakaria, Mohamad Pauzi, Ho, Yu Bin, Abdul Latif, Puziah, Saari, Nazamid
Format: Patent
Published: 2012
Online Access:http://psasir.upm.edu.my/id/eprint/33061/
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spelling my.upm.eprints.330612014-12-23T06:44:56Z http://psasir.upm.edu.my/id/eprint/33061/ Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids Zakaria, Mohamad Pauzi Ho, Yu Bin Abdul Latif, Puziah Saari, Nazamid A new method is developed to determine veterinary antibiotics and hormone in solid environmental samples by high performance liquid chromatography combined with tandem mass spectrometry (HPLC-MS/MS) using isotope dilution and internal standard quantitation techniques. This method has been developed particularly for simultaneous determination and quantification of nine antibiotics (doxycycline, erythromycin, enrofloxacin, flumequine, norfloxacin, sulfadizine, tilmicosin, trimethoprim and tylosin) and one hormone (progesterone) in animal manure, soil, and compost matrices. The developed method is based on solid phase extraction (SPE) followed by instrumental analysis using liquid chromatography electrospray ionization-tandem mass spectrometry (LC–ESI-MS/MS) with 25 minutes total run time. 2012-02-15 Patent NonPeerReviewed Mohamad Pauzi Zakaria (2012) Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids. PI2012000685.
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
description A new method is developed to determine veterinary antibiotics and hormone in solid environmental samples by high performance liquid chromatography combined with tandem mass spectrometry (HPLC-MS/MS) using isotope dilution and internal standard quantitation techniques. This method has been developed particularly for simultaneous determination and quantification of nine antibiotics (doxycycline, erythromycin, enrofloxacin, flumequine, norfloxacin, sulfadizine, tilmicosin, trimethoprim and tylosin) and one hormone (progesterone) in animal manure, soil, and compost matrices. The developed method is based on solid phase extraction (SPE) followed by instrumental analysis using liquid chromatography electrospray ionization-tandem mass spectrometry (LC–ESI-MS/MS) with 25 minutes total run time.
format Patent
author Zakaria, Mohamad Pauzi
Ho, Yu Bin
Abdul Latif, Puziah
Saari, Nazamid
spellingShingle Zakaria, Mohamad Pauzi
Ho, Yu Bin
Abdul Latif, Puziah
Saari, Nazamid
Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
author_facet Zakaria, Mohamad Pauzi
Ho, Yu Bin
Abdul Latif, Puziah
Saari, Nazamid
author_sort Zakaria, Mohamad Pauzi
title Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
title_short Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
title_full Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
title_fullStr Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
title_full_unstemmed Method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
title_sort method for simultaneous quantification of veterinary antibiotics and hormones in soil and biosolids
publishDate 2012
url http://psasir.upm.edu.my/id/eprint/33061/
_version_ 1643830769763745792
score 13.160551

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