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Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.

A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response...

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Main Authors: Fard Masoumi, Hamid Reza, Kassim, Anuar, Basri, Mahiran, Abdullah, Dzulkefly Kuang
Format: Article
Language:English
English
Published: MDPI 2011
Online Access:http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf
http://psasir.upm.edu.my/id/eprint/24951/
http://www.mdpi.com/
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spelling my.upm.eprints.249512015-09-18T08:19:40Z http://psasir.upm.edu.my/id/eprint/24951/ Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. Fard Masoumi, Hamid Reza Kassim, Anuar Basri, Mahiran Abdullah, Dzulkefly Kuang A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%. MDPI 2011-06-03 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf Fard Masoumi, Hamid Reza and Kassim, Anuar and Basri, Mahiran and Abdullah, Dzulkefly Kuang (2011) Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. Molecules, 16 (6). pp. 4672-4680. ISSN 1431-5157; ESSN:1420-3049 http://www.mdpi.com/ 10.3390/molecules16064672 English
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
English
description A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%.
format Article
author Fard Masoumi, Hamid Reza
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkefly Kuang
spellingShingle Fard Masoumi, Hamid Reza
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkefly Kuang
Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
author_facet Fard Masoumi, Hamid Reza
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkefly Kuang
author_sort Fard Masoumi, Hamid Reza
title Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
title_short Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
title_full Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
title_fullStr Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
title_full_unstemmed Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
title_sort determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (tea)-based esterquat cationic surfactant by a taguchi robust design method.
publisher MDPI
publishDate 2011
url http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf
http://psasir.upm.edu.my/id/eprint/24951/
http://www.mdpi.com/
_version_ 1643828513613021184
score 13.209306

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