Optimization of ultrasound-assisted oil extraction from Carica candamarcensis

• Main Authors: Sebayang A.H., Ideris F., Silitonga A.S., Shamsuddin A.H., Zamri M.F.M.A., Pulungan M.A., Siahaan S., Alfansury M., Kusumo F., Milano J.
• Other Authors: 39262519300
• Format: Article
• Published: Elsevier Ltd 2024
• Subjects: Alternative fuel; Biodiesel; Box-Behnken design; Carica candamarcensis; Response surface methodology; Ultrasound-assisted transesterification; Extraction; Fatty acids; Gas chromatography; Oils and fats; Physicochemical properties; Potassium hydroxide; Regression analysis; Surface properties; Transesterification; Tropics; Ultrasonics; Biodiesel production; Oil extraction; Optimisations; Physicochemical property; Process parameters; Response-surface methodology; Transesterifications; biofuel; catalysis; catalyst; dicotyledon; experimental study; extraction method; fatty acid; physicochemical property; solvent

This study focuses on the optimization of ultrasound-assisted oil extraction from Carica candamarcensis seed using response surface methodology. The process parameters considered were extraction time (30�60 min), ultrasound amplitude level (20�40%), and solvent to seed ratio (10�20 mL/g). These were varied as suggested by Box-Behnken experimental model. Optimum values of these process parameters were given by the regression model, with the corresponding extraction yield. The model was validated experimentally to ensure its reliability. Physicochemical properties and fatty acid compositions of the extracted oil were evaluated accordingly. Furthermore, the extracted oil was then converted into biodiesel via ultrasound-assisted transesterification, using potassium hydroxide as the catalyst. FAME contents of the produced biodiesel were measured using gas chromatography. In addition, physicochemical properties of the biodiesel were also determined accordingly. Hence, findings from this study would be beneficial in further exploration on the usage of Carica candamarcensis as a potential feedstock for biodiesel production. � 2023 Elsevier Ltd