Synthesis of carbide lime derived strong base catalyst for biodiesel production
Biodiesel; Calcium carbonate; Calcium fluoride; Carbon dioxide; Esters; Fatty acids; Fourier transform infrared spectroscopy; Hydrated lime; Lime; Morphology; Palm oil; Potassium compounds; Scanning electron microscopy; Sunflower oil; Temperature programmed desorption; Transesterification; Base cata...
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Trans Tech Publications Ltd
2023
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my.uniten.dspace-264412023-05-29T17:10:33Z Synthesis of carbide lime derived strong base catalyst for biodiesel production Lim H.H. Pua F.L. Rohaya O. Taufiq-Yap Y.H. Sharifah N. 57361566000 36024192100 57361480600 57194506693 57361566100 Biodiesel; Calcium carbonate; Calcium fluoride; Carbon dioxide; Esters; Fatty acids; Fourier transform infrared spectroscopy; Hydrated lime; Lime; Morphology; Palm oil; Potassium compounds; Scanning electron microscopy; Sunflower oil; Temperature programmed desorption; Transesterification; Base catalyst; Base strength; Biodiesel production; Carbide lime; Catalyst loadings; Structure and morphology; Temperature-programmed desorptions; Test temperatures; Transesterifications; ]+ catalyst; Catalysts Carbide lime is a result of acetylene production. Carbide lime made out of calcium hydroxide with a minor amount of calcium carbonate. In this study, carbide lime was used as the raw material to synthesize a new base catalyst with high base strength. A strong base catalyst was prepared through calcination and impregnation with potassium fluoride. The structure and morphology of catalyst were investigated by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM) The base strength was determined by Hammett Indicator test, temperature-programmed desorption of carbon dioxide (TPD-CO2). The surface area of the catalyst was determined by Brunauer-Emmet-Teller isotherm (BET). The catalytic performance was examined through a transesterification reaction. Fatty acid methyl ester (FAME) was successfully synthesized with the presence of carbide lime derived catalyst. The highest biodiesel conversion rate for sunflower oil was 95.83% with 6 wt% of catalyst loading, while palm oil was 88.07% with 3 wt% of catalyst loading. The presence of the ester functional group was determined by Fourier Transform Infrared Spectroscopy (FTIR) analysis. � 2021 Trans Tech Publications Ltd, Switzerland. Final 2023-05-29T09:10:33Z 2023-05-29T09:10:33Z 2021 Conference Paper 10.4028/www.scientific.net/SSP.317.251 2-s2.0-85120535364 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85120535364&doi=10.4028%2fwww.scientific.net%2fSSP.317.251&partnerID=40&md5=e7e8844c13d6529237f45c6d530e5e5d https://irepository.uniten.edu.my/handle/123456789/26441 317 SSP 251 256 Trans Tech Publications Ltd Scopus |
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| description |
Biodiesel; Calcium carbonate; Calcium fluoride; Carbon dioxide; Esters; Fatty acids; Fourier transform infrared spectroscopy; Hydrated lime; Lime; Morphology; Palm oil; Potassium compounds; Scanning electron microscopy; Sunflower oil; Temperature programmed desorption; Transesterification; Base catalyst; Base strength; Biodiesel production; Carbide lime; Catalyst loadings; Structure and morphology; Temperature-programmed desorptions; Test temperatures; Transesterifications; ]+ catalyst; Catalysts |
| author2 |
57361566000 |
| author_facet |
57361566000 Lim H.H. Pua F.L. Rohaya O. Taufiq-Yap Y.H. Sharifah N. |
| format |
Conference Paper |
| author |
Lim H.H. Pua F.L. Rohaya O. Taufiq-Yap Y.H. Sharifah N. |
| spellingShingle |
Lim H.H. Pua F.L. Rohaya O. Taufiq-Yap Y.H. Sharifah N. Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| author_sort |
Lim H.H. |
| title |
Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| title_short |
Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| title_full |
Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| title_fullStr |
Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| title_full_unstemmed |
Synthesis of carbide lime derived strong base catalyst for biodiesel production |
| title_sort |
synthesis of carbide lime derived strong base catalyst for biodiesel production |
| publisher |
Trans Tech Publications Ltd |
| publishDate |
2023 |
| _version_ |
1806426302785257472 |
| score |
13.214268 |