Sinterability of forsterite prepared via solid-state reaction
Olivine; Powders; Scanning electron microscopy; Sintering; Solid state reactions; Vickers hardness; Forsterite ceramics; Forsterite powder; Maximum relative density; Microstructural examination; Relative density; Scanning electron micrographs; Sintered samples; Synthesized powder; Fracture toughness
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2023
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my.uniten.dspace-224082023-05-29T14:00:47Z Sinterability of forsterite prepared via solid-state reaction Tan C.Y. Singh R. Teh Y.C. Tan Y.M. Yap B.K. 16029485400 41061958200 55877640300 55877494100 26649255900 Olivine; Powders; Scanning electron microscopy; Sintering; Solid state reactions; Vickers hardness; Forsterite ceramics; Forsterite powder; Maximum relative density; Microstructural examination; Relative density; Scanning electron micrographs; Sintered samples; Synthesized powder; Fracture toughness In this work, the sinterability of forsterite powder synthesized via solid-state reaction was investigated. X-ray diffraction (XRD) analyses indicate that the synthesized powder possessed peaks that correspond to stoichiometric forsterite. Scanning electron micrographs revealed that the powders were formed agglomerates, which were made up of loosely packed fine particles. Subsequently, the forsterite powders were cold isostatically pressed into a disk shape under 200 MPa and sintered in air at temperature ranging from 1200�C to 1500�C (interval of 50�C) with ramp rate of 10�C/min and dwelling time of 2 h. The sinterability of each sintered samples was examined in terms of phase stability, relative density, Vickers hardness, fracture toughness, and microstructural examination. XRD examination on all the sintered samples exhibited pure forsterite, in which the generated peaks were found to be in a good agreement with JCPDS card no. 34-0189. The densification of forsterite progressed to reach a maximum relative density of ~91% at 1500�C. This study also revealed that high-strength forsterite ceramic can be synthesized via solid-state reaction as forsterite attained favorable mechanical properties, having fracture toughness of 4.88 MPam1/2 and hardness of 7.11 GPa at 1400�C. � 2013 The American Ceramic Society. Final 2023-05-29T06:00:47Z 2023-05-29T06:00:47Z 2015 Article 10.1111/ijac.12172 2-s2.0-84924221213 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84924221213&doi=10.1111%2fijac.12172&partnerID=40&md5=84655cd06e0a4b9a03f81f3770c9e9c0 https://irepository.uniten.edu.my/handle/123456789/22408 12 2 437 442 Scopus |
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| description |
Olivine; Powders; Scanning electron microscopy; Sintering; Solid state reactions; Vickers hardness; Forsterite ceramics; Forsterite powder; Maximum relative density; Microstructural examination; Relative density; Scanning electron micrographs; Sintered samples; Synthesized powder; Fracture toughness |
| author2 |
16029485400 |
| author_facet |
16029485400 Tan C.Y. Singh R. Teh Y.C. Tan Y.M. Yap B.K. |
| format |
Article |
| author |
Tan C.Y. Singh R. Teh Y.C. Tan Y.M. Yap B.K. |
| spellingShingle |
Tan C.Y. Singh R. Teh Y.C. Tan Y.M. Yap B.K. Sinterability of forsterite prepared via solid-state reaction |
| author_sort |
Tan C.Y. |
| title |
Sinterability of forsterite prepared via solid-state reaction |
| title_short |
Sinterability of forsterite prepared via solid-state reaction |
| title_full |
Sinterability of forsterite prepared via solid-state reaction |
| title_fullStr |
Sinterability of forsterite prepared via solid-state reaction |
| title_full_unstemmed |
Sinterability of forsterite prepared via solid-state reaction |
| title_sort |
sinterability of forsterite prepared via solid-state reaction |
| publishDate |
2023 |
| _version_ |
1806426275853631488 |
| score |
13.214268 |