Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution Impregnated Pulai (Alstonia spp.) Wood Using Response Surface Methodology
Significant effects of organoclay and poly(melamine-co-formaldehyde)- methylated (PMFM) impregnation on the mechanical, morphological, and thermal characteristics of raw pulai wood were investigated in this work. The material’s modulus of elasticity (MOE) as well as the maximum compression force (M...
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my.unimas.ir.395552022-10-04T03:37:42Z http://ir.unimas.my/id/eprint/39555/ Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution Impregnated Pulai (Alstonia spp.) Wood Using Response Surface Methodology Perry Law, Nyuk Khui Md. Rezaur, Rahman Hafizah, Abdul Halim Yun Durul, Huda Sinin, Hamdan Muhammad Khusairy, Bakri Mohammad Mahbubul, Matin Kuok King, Kuok Chin Mei, Yun Abdullah S, Al-Bogami Khalid A., Alamry Mohammed M., Rahman TP Chemical technology Significant effects of organoclay and poly(melamine-co-formaldehyde)- methylated (PMFM) impregnation on the mechanical, morphological, and thermal characteristics of raw pulai wood were investigated in this work. The material’s modulus of elasticity (MOE) as well as the maximum compression force (MCF) of the impregnated organoclay/PMFM pulai wood samples were optimized using a designed experiment. The MOE and MCF models had R2 values of 0.9228 and 0.8340, respectively. After the impregnation of organoclay/PMFM pulai wood samples, the MOE and MCF increased considerably, indicating that the pulai wood's mechanical characteristics had improved. The compositional analysis verified the polymerization and dispersion of organoclay and PMFM. Using Fourier transform infrared spectroscopy, reduction in the hydroxyl groups was detected. The impregnated organoclay/PMFM pulai wood samples had successfully filled the pores and cell cavities, as seen by scanning electron microscopy. The thermal stability of the impregnated organoclay/PMFM pulai wood samples was better than that of the raw pulai wood, with a higher glass transition temperature as determined by differential scanning calorimetry. The thermogravimetric study revealed that the impregnated organoclay/PMFM pulai wood samples had higher decomposition temperatures than the raw pulai wood sample. BioResources 2022 Article PeerReviewed text en http://ir.unimas.my/id/eprint/39555/1/Characterization.pdf Perry Law, Nyuk Khui and Md. Rezaur, Rahman and Hafizah, Abdul Halim Yun and Durul, Huda and Sinin, Hamdan and Muhammad Khusairy, Bakri and Mohammad Mahbubul, Matin and Kuok King, Kuok and Chin Mei, Yun and Abdullah S, Al-Bogami and Khalid A., Alamry and Mohammed M., Rahman (2022) Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution Impregnated Pulai (Alstonia spp.) Wood Using Response Surface Methodology. BioResources, 17 (2). pp. 2780-2809. ISSN 1930-2126 https://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_17_2_2780_Nyuk_Khui_Optimization_Organoclay_Pulai_Wood DOI: 10.15376/biores.17.2.2780-2809 |
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TP Chemical technology Perry Law, Nyuk Khui Md. Rezaur, Rahman Hafizah, Abdul Halim Yun Durul, Huda Sinin, Hamdan Muhammad Khusairy, Bakri Mohammad Mahbubul, Matin Kuok King, Kuok Chin Mei, Yun Abdullah S, Al-Bogami Khalid A., Alamry Mohammed M., Rahman Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution Impregnated Pulai (Alstonia spp.) Wood Using Response Surface Methodology |
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Significant effects of organoclay and poly(melamine-co-formaldehyde)- methylated (PMFM) impregnation on the mechanical, morphological, and thermal characteristics of raw pulai wood were investigated in this work.
The material’s modulus of elasticity (MOE) as well as the maximum compression force (MCF) of the impregnated organoclay/PMFM pulai wood samples were optimized using a designed experiment. The MOE and MCF models had R2 values of 0.9228 and 0.8340, respectively. After the impregnation of organoclay/PMFM pulai wood samples, the MOE and MCF increased considerably, indicating that the pulai wood's mechanical characteristics had improved. The compositional analysis verified the polymerization and dispersion of organoclay and PMFM. Using Fourier transform infrared spectroscopy, reduction in the hydroxyl groups was
detected. The impregnated organoclay/PMFM pulai wood samples had successfully filled the pores and cell cavities, as seen by scanning electron microscopy. The thermal stability of the impregnated organoclay/PMFM pulai wood samples was better than that of the raw pulai wood, with a higher glass transition temperature as determined by differential scanning calorimetry. The thermogravimetric study revealed that the impregnated organoclay/PMFM pulai wood samples had higher decomposition temperatures than the raw pulai wood sample. |
format |
Article |
author |
Perry Law, Nyuk Khui Md. Rezaur, Rahman Hafizah, Abdul Halim Yun Durul, Huda Sinin, Hamdan Muhammad Khusairy, Bakri Mohammad Mahbubul, Matin Kuok King, Kuok Chin Mei, Yun Abdullah S, Al-Bogami Khalid A., Alamry Mohammed M., Rahman |
author_facet |
Perry Law, Nyuk Khui Md. Rezaur, Rahman Hafizah, Abdul Halim Yun Durul, Huda Sinin, Hamdan Muhammad Khusairy, Bakri Mohammad Mahbubul, Matin Kuok King, Kuok Chin Mei, Yun Abdullah S, Al-Bogami Khalid A., Alamry Mohammed M., Rahman |
author_sort |
Perry Law, Nyuk Khui |
title |
Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution
Impregnated Pulai (Alstonia spp.) Wood Using
Response Surface Methodology |
title_short |
Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution
Impregnated Pulai (Alstonia spp.) Wood Using
Response Surface Methodology |
title_full |
Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution
Impregnated Pulai (Alstonia spp.) Wood Using
Response Surface Methodology |
title_fullStr |
Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution
Impregnated Pulai (Alstonia spp.) Wood Using
Response Surface Methodology |
title_full_unstemmed |
Characterization and Optimization of Organoclaypoly(melamine-co-formaldehyde)-methylated Solution
Impregnated Pulai (Alstonia spp.) Wood Using
Response Surface Methodology |
title_sort |
characterization and optimization of organoclaypoly(melamine-co-formaldehyde)-methylated solution
impregnated pulai (alstonia spp.) wood using
response surface methodology |
publisher |
BioResources |
publishDate |
2022 |
url |
http://ir.unimas.my/id/eprint/39555/1/Characterization.pdf http://ir.unimas.my/id/eprint/39555/ https://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_17_2_2780_Nyuk_Khui_Optimization_Organoclay_Pulai_Wood |
_version_ |
1746213623481499648 |
score |
13.19449 |