Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays

International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia.

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Main Authors: Lai, Chin Wei, Srimala, Sreekantan
Other Authors: stevenlai5275@yahoo.com
Format: Article
Language:English
Published: Universiti Malaysia Perlis 2010
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Online Access:http://dspace.unimap.edu.my/xmlui/handle/123456789/9011
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spelling my.unimap-90112010-08-23T06:02:37Z Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays Lai, Chin Wei Srimala, Sreekantan stevenlai5275@yahoo.com Titania nanotube Cleaning agent Photocatalytic activity International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI) International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia. Titania nanotube arrays were synthesized by anodizing Ti foil in ethylene glycol (EG) containing ammonium fluoride (NH4F). The role of fluoride ion and the different cleaning agents were investigated. The morphology was observed via Field Emission Scanning Electron Microscopy (FESEM). A self-organized TiO2 nanotube with an average inner diameter of 110 nm and length of 9.5 μm was acquired by anodizing the foil at 60 V for 60 minutes. The presence of F- ions leads to chemical dissolution of Ti oxide layer. The chemical dissolution rate increased with increasing the fluoride content because more F- ion is available to attack the barrier layer. When the barrier layer gets thinner the oxidation rate will increase and thus formed the long tubes. Acetone and DI water were used as a cleaning agent. It was found that sample washed in acetone and ultrasonic for 1 minute, the precipitates like oxide layer formed onto surface of the nanotubes was successfully removed and revealed smooth and clean pores. Such clear opening enhanced the photocatalytic activity of methyl orange degradation because the diffusion of methyl orange takes place not only on the outer surface of TiO2 nanotube but also on the inner walls. 2010-08-23T06:02:37Z 2010-08-23T06:02:37Z 2010-06-09 Article p.29-32 978-967-5760-02-0 http://hdl.handle.net/123456789/9011 en Proceedings of the International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI2010) Universiti Malaysia Perlis School of Materials Engineering & School of Environmental Engineering
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic Titania nanotube
Cleaning agent
Photocatalytic activity
International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI)
spellingShingle Titania nanotube
Cleaning agent
Photocatalytic activity
International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI)
Lai, Chin Wei
Srimala, Sreekantan
Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
description International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia.
author2 stevenlai5275@yahoo.com
author_facet stevenlai5275@yahoo.com
Lai, Chin Wei
Srimala, Sreekantan
format Article
author Lai, Chin Wei
Srimala, Sreekantan
author_sort Lai, Chin Wei
title Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
title_short Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
title_full Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
title_fullStr Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
title_full_unstemmed Effect of fluoride content and cleaning agent on the formation of self organized TiO2 nanotube arrays
title_sort effect of fluoride content and cleaning agent on the formation of self organized tio2 nanotube arrays
publisher Universiti Malaysia Perlis
publishDate 2010
url http://dspace.unimap.edu.my/xmlui/handle/123456789/9011
_version_ 1643789348760453120
score 13.223943