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Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics

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Main Authors: Abdelhalim, Elbasset, Tajddin., Lamcharfi, Farid Abdi, Hicham, Laribou, Abdelhak Elghandouri, Lamiae Mrharrab
Other Authors: elbasset.abdelhalim@gmail.com
Format: Article
Language:English
Published: Universiti Malaysia Perlis (UniMAP) 2022
Subjects:
Band gap energy
Low dielectric loss
Phase formation
Raman spectroscopy
SrTiO3
X-ray diffraction
Online Access:http://dspace.unimap.edu.my:80/xmlui/handle/123456789/77141
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spelling my.unimap-771412022-11-23T03:42:30Z Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics Abdelhalim, Elbasset Abdelhalim, Elbasset Tajddin., Lamcharfi Farid Abdi Hicham, Laribou Abdelhak Elghandouri Lamiae Mrharrab elbasset.abdelhalim@gmail.com abdelhalim.elbasset@usmba.ac.ma LSSC, Department of Electrical Engineering, Faculty of Science and Technology (FST) B.P.2202, University Sidi Mohamed Ben Abdellah Laboratory of Physics, Theoretical and Applied, FSDM B.P. 179 Laboratory for microstructures and materials mechanics. University of Lorraine Band gap energy Low dielectric loss Phase formation Raman spectroscopy SrTiO3 X-ray diffraction Link to publisher's homepage at http://ijneam.unimap.edu.my/ The aim of this work is to investigate the effect of calcination temperature (600, 700 and 800°C) and sintering temperature (1000, 1050 and 1100°C) on pure phase formation, microstructure and dielectric properties of perovskite SrTiO3 (ST) ceramics. The results show that the calcination conditions at 600°C for 6h, are sufficient to obtain this phase. Furthermore, lattice parameter (a) tends to increase with increasing calcinations temperature. The Raman spectroscopy characterization indicates the presence in the calcination spectrum at 600°C of extra-modes located around 113 and 617 cm-1. The optical absorption edge of SrTiO3 was explored in the temperature from 200 to 1000°C. The results suggest that the band gap energy is increasing with temperature. On the other hand, the results found show that the average grain size of the sintered ST at 1100°C is the order of 12µm which is respectively larger than that at 1000 (~ 3.2µm) and at 1050°C (~ 6.4µm). The dielectric study shows that samples sintered at 1100°C have smaller and stable dielectric losses as a function of frequency. 2022 2022-11-23T03:42:30Z 2022-11-23T03:42:30Z 2022-10 Article International Journal of Nanoelectronics and Materials, vol.15 (4), 2022, pages 331-342 1985-5761 (Printed) 1997-4434 (Online) http://dspace.unimap.edu.my:80/xmlui/handle/123456789/77141 http://ijneam.unimap.edu.my en Universiti Malaysia Perlis (UniMAP)
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic Band gap energy
Low dielectric loss
Phase formation
Raman spectroscopy
SrTiO3
X-ray diffraction
spellingShingle Band gap energy
Low dielectric loss
Phase formation
Raman spectroscopy
SrTiO3
X-ray diffraction
Abdelhalim, Elbasset
Abdelhalim, Elbasset
Tajddin., Lamcharfi
Farid Abdi
Hicham, Laribou
Abdelhak Elghandouri
Lamiae Mrharrab
Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
description Link to publisher's homepage at http://ijneam.unimap.edu.my/
author2 elbasset.abdelhalim@gmail.com
author_facet elbasset.abdelhalim@gmail.com
Abdelhalim, Elbasset
Abdelhalim, Elbasset
Tajddin., Lamcharfi
Farid Abdi
Hicham, Laribou
Abdelhak Elghandouri
Lamiae Mrharrab
format Article
author Abdelhalim, Elbasset
Abdelhalim, Elbasset
Tajddin., Lamcharfi
Farid Abdi
Hicham, Laribou
Abdelhak Elghandouri
Lamiae Mrharrab
author_sort Abdelhalim, Elbasset
title Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
title_short Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
title_full Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
title_fullStr Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
title_full_unstemmed Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
title_sort correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of srtio3 ceramics
publisher Universiti Malaysia Perlis (UniMAP)
publishDate 2022
url http://dspace.unimap.edu.my:80/xmlui/handle/123456789/77141
_version_ 1753972987634122752
score 13.214268

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