Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis

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Main Author: Nor Atikah, Ab Rahman
Other Authors: Sam Sung, Ting, Dr.
Format: Learning Object
Language:English
Published: Universiti Malaysia Perlis (UniMAP) 2021
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Online Access:http://dspace.unimap.edu.my:80/xmlui/handle/123456789/73695
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spelling my.unimap-736952022-01-25T01:44:00Z Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis Nor Atikah, Ab Rahman Sam Sung, Ting, Dr. School of Bioprocess Engineering Empty fruit bunch (EFB) Wastes Nanocellulose Nanocrystalline cellulose (NCC) Access is limited to UniMAP community. Empty fruit bunch is one of the most abundant lignocellulosic wastes and has a potential in producing nanocellulose for various uses. In this study, an alkaline pre-treatment and acid hydrolysis are the most important process were utilized for the production of nanocrystalline cellulose, NCC. At first stage, EFB powder was first treated with 4 wt% sodium hydroxide (NaOH) solution at 80 ̊C at 2 hours. The treated EFB fibres then was bleached with 1.7 wt% sodium chlorite (NaClO2) solution, acetate buffer and distilled water at 70 ̊C-80 ̊C for 2 hours following with acid hydrolysis. At his stages, clear milky solution produced was introduced as Nanocrystalline cellulose. The optimization has been carried out by using Box-Behnken under RSM to analyze the effect of acid concentration, reaction temperature and reaction time on production of NCC yields. From the model response, the optimum NCCs yield produced is 17.52%. While, the optimum condition acid concentration, reaction temperature and reaction time were at 64.81%w/w, 60 ⁰C and 43.03min respectively. Through this experiment, nanocrystalline cellulose are successfully produced by acid hydrolysis. 2021 2022-01-25T01:44:00Z 2022-01-25T01:44:00Z 2017-06 Learning Object http://dspace.unimap.edu.my:80/xmlui/handle/123456789/73695 en Universiti Malaysia Perlis (UniMAP)
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic Empty fruit bunch (EFB)
Wastes
Nanocellulose
Nanocrystalline cellulose (NCC)
spellingShingle Empty fruit bunch (EFB)
Wastes
Nanocellulose
Nanocrystalline cellulose (NCC)
Nor Atikah, Ab Rahman
Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
description Access is limited to UniMAP community.
author2 Sam Sung, Ting, Dr.
author_facet Sam Sung, Ting, Dr.
Nor Atikah, Ab Rahman
format Learning Object
author Nor Atikah, Ab Rahman
author_sort Nor Atikah, Ab Rahman
title Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
title_short Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
title_full Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
title_fullStr Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
title_full_unstemmed Preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
title_sort preparation, characterization and optimization of empty fruit bunch nanocrystalline cellulose (ncc) by acid hydroysis
publisher Universiti Malaysia Perlis (UniMAP)
publishDate 2021
url http://dspace.unimap.edu.my:80/xmlui/handle/123456789/73695
_version_ 1729704651694014464
score 13.214268