Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method
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my.unimap-677112020-09-28T02:59:24Z Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method Ziad, T. Khodiar Nadir, F. Habubi Intessar, K. Abd Ahmed, M. Shano nadirfadhil@uomustansiriyah.edu.iq Cu1-xAlxO Sol-gel method Structural properties Link to publisher's homepage at http://ijneam.unimap.edu.my In this study, the sol-gel process has been adopted for the synthesis of Cu1-xAlxO nanostructures (0≤ x ≤ 0.90, in steps of 0.10). The system revealed pure CuO phase with monoclinic structure. Al2O3 phase and copper oxide (Cu2O) were developed at higher substituent concentrations till x=0.40. Structural properties were studied by X-ray diffraction (XRD) and morphological properties by Scanning Electron Microscope (SEM). Average crystallite size from the range of 12.65 nm to 22.9 nm was calculated by Scherer formula. The SEM images indicated that the Cu1-xAlxO possessed nanoparticles like structure, i.e. it contained some pores or voids and vacancies caused by a difference in experimental conditions. Results of EDX revealed the presence of Aluminum (Al), oxygen (O) and copper (Cu) elements in Cu1-xAlxO and the data showed that the nanoparticles were nearly stoichiometric. 2020-09-28T02:59:24Z 2020-09-28T02:59:24Z 2020-07 Article International Journal of Nanoelectronics and Materials, vol.13(3), 2020, pages 433-444 1985-5761 (Printed) 1997-4434 (Online) http://dspace.unimap.edu.my:80/xmlui/handle/123456789/67711 http://ijneam.unimap.edu.my en Universiti Malaysia Perlis (UniMAP) |
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Cu1-xAlxO Sol-gel method Structural properties Ziad, T. Khodiar Nadir, F. Habubi Intessar, K. Abd Ahmed, M. Shano Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
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Link to publisher's homepage at http://ijneam.unimap.edu.my |
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nadirfadhil@uomustansiriyah.edu.iq |
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nadirfadhil@uomustansiriyah.edu.iq Ziad, T. Khodiar Nadir, F. Habubi Intessar, K. Abd Ahmed, M. Shano |
format |
Article |
author |
Ziad, T. Khodiar Nadir, F. Habubi Intessar, K. Abd Ahmed, M. Shano |
author_sort |
Ziad, T. Khodiar |
title |
Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
title_short |
Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
title_full |
Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
title_fullStr |
Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
title_full_unstemmed |
Structural and morphological properties of Cu1-xAlxO nanostructures prepared by sol-gel method |
title_sort |
structural and morphological properties of cu1-xalxo nanostructures prepared by sol-gel method |
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Universiti Malaysia Perlis (UniMAP) |
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2020 |
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http://dspace.unimap.edu.my:80/xmlui/handle/123456789/67711 |
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1698698355835666432 |
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13.222552 |