Cover Image

Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method

Link to publisher's homepage at http://ijneam.unimap.edu.my

Saved in:
Bibliographic Details
Main Authors: Zakiyyu, I. Takai, Mohd K. Mustafa, Saliza, Asman, Khairunnadim, A. Sekak
Other Authors: zitakai21@gmail.com
Format: Article
Language:English
Published: Universiti Malaysia Perlis (UniMAP) 2019
Subjects:
Sol-Gel Method
Magnetite Nanoparticles
Particles Size
Morphologies
XRD
Online Access:http://dspace.unimap.edu.my:80/xmlui/handle/123456789/58784
Tags: Add Tag
No Tags, Be the first to tag this record!
id my.unimap-58784
record_format dspace
spelling my.unimap-587842019-03-06T09:54:28Z Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method Zakiyyu, I. Takai Mohd K. Mustafa Saliza, Asman Khairunnadim, A. Sekak zitakai21@gmail.com Sol-Gel Method Magnetite Nanoparticles Particles Size Morphologies XRD Link to publisher's homepage at http://ijneam.unimap.edu.my The magnetite (Fe3O4) nanoparticles were successfully synthesized and annealed under vacuum at different temperature. The Fe3O4 nanoparticles prepared via sol-gel assisted method and annealed at 200-400ºC were characterized by Fourier Transformation Infrared Spectroscopy (FTIR), X-ray Diffraction spectra (XRD), Field Emission Scanning Electron Microscope (FESEM) and Atomic Force Microscopy (AFM). The XRD result indicate the presence of Fe3O4 nanoparticles, and the Scherer`s Formula calculated the mean particles size in range of 2-25 nm. The FESEM result shows that the morphologies of the particles annealed at 400ºC are more spherical and partially agglomerated, while the EDS result indicates the presence of Fe3O4 by showing Fe-O group of elements. AFM analyzed the 3D and roughness of the sample; the Fe3O4 nanoparticles have a minimum diameter of 79.04 nm, which is in agreement with FESEM result. In many cases, the synthesis of Fe3O4 nanoparticles using FeCl3 and FeCl2 has not been achieved, according to some literatures, but this research was able to obtained Fe3O4 nanoparticles base on the characterization results. 2019-03-06T09:54:28Z 2019-03-06T09:54:28Z 2019-01 Article International Journal of Nanoelectronics and Materials, vol.12(1), 2019, pages 37-46 1985-5761 (Printed) 1997-4434 (Online) http://dspace.unimap.edu.my:80/xmlui/handle/123456789/58784 en Universiti Malaysia Perlis (UniMAP)
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic Sol-Gel Method
Magnetite Nanoparticles
Particles Size
Morphologies
XRD
spellingShingle Sol-Gel Method
Magnetite Nanoparticles
Particles Size
Morphologies
XRD
Zakiyyu, I. Takai
Mohd K. Mustafa
Saliza, Asman
Khairunnadim, A. Sekak
Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
description Link to publisher's homepage at http://ijneam.unimap.edu.my
author2 zitakai21@gmail.com
author_facet zitakai21@gmail.com
Zakiyyu, I. Takai
Mohd K. Mustafa
Saliza, Asman
Khairunnadim, A. Sekak
format Article
author Zakiyyu, I. Takai
Mohd K. Mustafa
Saliza, Asman
Khairunnadim, A. Sekak
author_sort Zakiyyu, I. Takai
title Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
title_short Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
title_full Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
title_fullStr Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
title_full_unstemmed Preparation and Characterization of Magnetite (Fe3O4) nanoparticles By Sol-Gel Method
title_sort preparation and characterization of magnetite (fe3o4) nanoparticles by sol-gel method
publisher Universiti Malaysia Perlis (UniMAP)
publishDate 2019
url http://dspace.unimap.edu.my:80/xmlui/handle/123456789/58784
_version_ 1643805993574858752
score 13.214268

Similar Items