Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication

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Main Authors: Sodipo, Bashiru Kayode, Azlan, Abdul Aziz, Munira, Mustapa
Other Authors: bashirsodipo@gmail.com.
Format: Article
Language:English
Published: Universiti Malaysia Perlis 2016
Subjects:
GNP
Online Access:http://dspace.unimap.edu.my:80/xmlui/handle/123456789/41310
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spelling my.unimap-413102017-11-21T02:01:01Z Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication Sodipo, Bashiru Kayode Azlan, Abdul Aziz Munira, Mustapa bashirsodipo@gmail.com. lan@usm.my. munirahmostapa@yahoo.com. SPION GNP APTES CORE-SHELL GNP coated SPION Link to publisher's homepage at http://ijneam.unimap.edu.my/ We reported a simple protocol for synthesizing small-scale gold coated superparamagnetic iron oxide nanoparticles (SPION). The synthesis of the core-shell nanoparticles of the SPION-gold nanoparticles (GNP) was through chemical reduction method in an ultrasonic field environment. The SPION was produced by co-precipitating iron (ii) and (iii) chloride salt in sodium chloride solution as a c o-precipitating agent. The surface of the SPION was sonochemically functionalized with a 3- aminopropyltriethoxysilane (APTES) which served as a linker. Gold precursor was chemically reduced with chilled sodium borohydride in the presence of the APTES functionalized SPION seed. The GNP covalently binds and assembles on the terminal amine groups on the SPION. Physical characterization with Energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction pattern (XRD) and Ultraviolet–visible spectroscopy (UV-Vis) confirmed the composite nanoparticles to be GNP coated SPION. 2016-04-22T07:50:34Z 2016-04-22T07:50:34Z 2015 Article International Journal of Nanoelectronics and Materials, vol.8 (1), 2015, pages 1-6 1985-5761 (Printed) 1997-4434 (Online) http://dspace.unimap.edu.my:80/xmlui/handle/123456789/41310 en Universiti Malaysia Perlis
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic SPION
GNP
APTES
CORE-SHELL
GNP coated SPION
spellingShingle SPION
GNP
APTES
CORE-SHELL
GNP coated SPION
Sodipo, Bashiru Kayode
Azlan, Abdul Aziz
Munira, Mustapa
Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
description Link to publisher's homepage at http://ijneam.unimap.edu.my/
author2 bashirsodipo@gmail.com.
author_facet bashirsodipo@gmail.com.
Sodipo, Bashiru Kayode
Azlan, Abdul Aziz
Munira, Mustapa
format Article
author Sodipo, Bashiru Kayode
Azlan, Abdul Aziz
Munira, Mustapa
author_sort Sodipo, Bashiru Kayode
title Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
title_short Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
title_full Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
title_fullStr Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
title_full_unstemmed Facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
title_sort facile synthesis and characteristics of gold coated superparamagnetic iron oxide nanoparticles via sonication
publisher Universiti Malaysia Perlis
publishDate 2016
url http://dspace.unimap.edu.my:80/xmlui/handle/123456789/41310
_version_ 1643802794709221376
score 13.222552