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Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid

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Main Authors: Rosniza, Hamzah, Mohamad, Abu Bakar, Prof., Nik Noriman, Zulkepli, Dr., Mohd Arif Anuar, Mohd Salleh, Mohd Mustafa Al-Bakri, Abdullah
Other Authors: rosniza.hamzah@gmail.com
Format: Article
Language:English
Published: Trans Tech Publications 2014
Subjects:
ENR-50
Epoxide ring opening
Hybrid
Silsequioxanes
Online Access:http://dspace.unimap.edu.my:80/dspace/handle/123456789/33142
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spelling my.unimap-331422014-03-26T07:21:32Z Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid Rosniza, Hamzah Mohamad, Abu Bakar, Prof. Nik Noriman, Zulkepli, Dr. Mohd Arif Anuar, Mohd Salleh Mohd Mustafa Al-Bakri, Abdullah rosniza.hamzah@gmail.com niknoriman@unimap.edu.my arifanuar@unimap.edu.my mustafa_albakri@unimap.edu.my ENR-50 Epoxide ring opening Hybrid Silsequioxanes Link to publisher's homepage at http://www.ttp.net/ A composite comprising cyclopentyl trisilanol siisesquioxanes (CpSSQ(OH)3) and 50% epoxidized natural rubber (ENR-50) was prepared at reflux temperature employed hydrochloric acid (HCl) as catalyst. HCl was found to be an effective catalyst to promote ring opening reaction of ENR-50 and tailored CpSSQ(OH)3 to the ENR-50 polymer chains via chemical reaction. FTIR spectroscopy reveals a hydroxyl stretching indicating the occurrence of epoxide ring opening reaction. !H NMR analysis further proved the incorporation of CpSSQ(OH)3 into ENR-50 polymer chains via shiftment of proton chemical shift and addition in the proton integrals. Si 29NMR analysis evidence the Si-O-C bond through a chemical shift of silanol group from CpSSQ(OH)3. 2014-03-26T07:21:32Z 2014-03-26T07:21:32Z 2013 Article Advanced Materials Research, vol. 795, 2013, pages 251-255 978-303785811-0 1022-6680 http://www.scientific.net/AMR.795.251 http://dspace.unimap.edu.my:80/dspace/handle/123456789/33142 en Trans Tech Publications
institution Universiti Malaysia Perlis
building UniMAP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Perlis
content_source UniMAP Library Digital Repository
url_provider http://dspace.unimap.edu.my/
language English
topic ENR-50
Epoxide ring opening
Hybrid
Silsequioxanes
spellingShingle ENR-50
Epoxide ring opening
Hybrid
Silsequioxanes
Rosniza, Hamzah
Mohamad, Abu Bakar, Prof.
Nik Noriman, Zulkepli, Dr.
Mohd Arif Anuar, Mohd Salleh
Mohd Mustafa Al-Bakri, Abdullah
Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
description Link to publisher's homepage at http://www.ttp.net/
author2 rosniza.hamzah@gmail.com
author_facet rosniza.hamzah@gmail.com
Rosniza, Hamzah
Mohamad, Abu Bakar, Prof.
Nik Noriman, Zulkepli, Dr.
Mohd Arif Anuar, Mohd Salleh
Mohd Mustafa Al-Bakri, Abdullah
format Article
author Rosniza, Hamzah
Mohamad, Abu Bakar, Prof.
Nik Noriman, Zulkepli, Dr.
Mohd Arif Anuar, Mohd Salleh
Mohd Mustafa Al-Bakri, Abdullah
author_sort Rosniza, Hamzah
title Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
title_short Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
title_full Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
title_fullStr Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
title_full_unstemmed Preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (CpSSQ(OH)3 - ENR-50) composite hybrid in the presence of HCI acid
title_sort preparation of cyciopentyi trisiianoi siisesquioxanes - modified natural rubber (cpssq(oh)3 - enr-50) composite hybrid in the presence of hci acid
publisher Trans Tech Publications
publishDate 2014
url http://dspace.unimap.edu.my:80/dspace/handle/123456789/33142
_version_ 1643797081515622400
score 13.214268

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