One-step electrochemical synthesis of MoS2/graphene composite for supercapacitor application
In this study, an MoS2/graphene composite is fabricated from bulk MoS2 and graphite rod via a facile electrochemical exfoliation method. The as-prepared samples are characterized by X-ray diffraction, field emission scanning electron microscopy, Fourier transform infrared spectroscopy and ultraviole...
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| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Springer Link
2019
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| Subjects: | |
| Online Access: | http://umpir.ump.edu.my/id/eprint/26951/1/One-step%20electrochemical%20synthesis%20of%20MoS2.pdf http://umpir.ump.edu.my/id/eprint/26951/ https://doi.org/10.1007/s10008-019-04449-5 https://doi.org/10.1007/s10008-019-04449-5 |
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| Summary: | In this study, an MoS2/graphene composite is fabricated from bulk MoS2 and graphite rod via a facile electrochemical exfoliation method. The as-prepared samples are characterized by X-ray diffraction, field emission scanning electron microscopy, Fourier transform infrared spectroscopy and ultraviolet-visible spectroscopy techniques to confirm the formation of the MoS2/graphene composite. The electrochemical behavior of the MoS2/graphene composite is evaluated through cyclic voltammetry, galvanostatic charge/discharge and electrochemical impedance spectroscopy. It exhibits high specific capacitance of 227 F g−1 as compared with the exfoliated graphene (85 F g−1) and exfoliated MoS2 (70 F g−1) at a current density of 0.1 A g−1. This can be attributed to the synergistic effect between graphene and MoS2. Moreover, it displays high electrochemical stability and low electrical resistance. |
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