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Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex

SBA-16 supported 1,2-diaminocyclohexane Pd-complex (100–500 mol ppm of Pd) was found to be an efficient catalyst in the palladium-catalyzed Mizoroki–Heck, Suzuki–Miyaura and copper-free Sonogashira cross-coupling reactions of aryl halides under mild reaction conditions. The Pd-complex efficiently pr...

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Main Authors: Sarkar, Shaheen M., Lutfor, M. R., M. M., Yusoff
Format: Article
Language:English
Published: Royal Society of Chemistry 2015
Subjects:
QD Chemistry
Online Access:http://umpir.ump.edu.my/id/eprint/12768/1/New%20J%20Chem.pdf
http://umpir.ump.edu.my/id/eprint/12768/
http://dx.doi.org/10.1039/C4NJ02319F
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spelling my.ump.umpir.127682018-02-14T04:00:41Z http://umpir.ump.edu.my/id/eprint/12768/ Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex Sarkar, Shaheen M. Lutfor, M. R. M. M., Yusoff QD Chemistry SBA-16 supported 1,2-diaminocyclohexane Pd-complex (100–500 mol ppm of Pd) was found to be an efficient catalyst in the palladium-catalyzed Mizoroki–Heck, Suzuki–Miyaura and copper-free Sonogashira cross-coupling reactions of aryl halides under mild reaction conditions. The Pd-complex efficiently promoted all of these coupling reactions with appropriate coupling partners to afford the corresponding coupling products with almost quantitative yield. The supported Pd-complex was readily recovered and used five times without a significant loss of its catalytic activity. Royal Society of Chemistry 2015 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/12768/1/New%20J%20Chem.pdf Sarkar, Shaheen M. and Lutfor, M. R. and M. M., Yusoff (2015) Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex. New Journal of Chemistry, 39 (5). pp. 3564-3570. ISSN 1144-0546 http://dx.doi.org/10.1039/C4NJ02319F DOI: 10.1039/C4NJ02319F
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Sarkar, Shaheen M.
Lutfor, M. R.
M. M., Yusoff
Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
description SBA-16 supported 1,2-diaminocyclohexane Pd-complex (100–500 mol ppm of Pd) was found to be an efficient catalyst in the palladium-catalyzed Mizoroki–Heck, Suzuki–Miyaura and copper-free Sonogashira cross-coupling reactions of aryl halides under mild reaction conditions. The Pd-complex efficiently promoted all of these coupling reactions with appropriate coupling partners to afford the corresponding coupling products with almost quantitative yield. The supported Pd-complex was readily recovered and used five times without a significant loss of its catalytic activity.
format Article
author Sarkar, Shaheen M.
Lutfor, M. R.
M. M., Yusoff
author_facet Sarkar, Shaheen M.
Lutfor, M. R.
M. M., Yusoff
author_sort Sarkar, Shaheen M.
title Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
title_short Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
title_full Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
title_fullStr Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
title_full_unstemmed Heck, Suzuki and Sonogashira Cross-coupling Reactions using ppm level of SBA-16 supported Pd-complex
title_sort heck, suzuki and sonogashira cross-coupling reactions using ppm level of sba-16 supported pd-complex
publisher Royal Society of Chemistry
publishDate 2015
url http://umpir.ump.edu.my/id/eprint/12768/1/New%20J%20Chem.pdf
http://umpir.ump.edu.my/id/eprint/12768/
http://dx.doi.org/10.1039/C4NJ02319F
_version_ 1643666988342444032
score 13.160551

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