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N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate

The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the ot...

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Main Authors: Yehye, W.A., Ariffin, A., Ng, S.W.
Format: Article
Published: International Union of Crystallography 2008
Subjects:
QD Chemistry
Online Access:http://eprints.um.edu.my/924/
http://www.ncbi.nlm.nih.gov/pubmed/21203167
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spelling my.um.eprints.9242019-01-31T02:01:55Z http://eprints.um.edu.my/924/ N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate Yehye, W.A. Ariffin, A. Ng, S.W. QD Chemistry The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the other Schiff base mol-ecule, the 2-hydr-oxy-substituted benzene ring is oriented so that the 2-hydr-oxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base mol-ecules inter-act with methanol solvent to furnish a hydrogen-bonded chain. International Union of Crystallography 2008 Article PeerReviewed Yehye, W.A. and Ariffin, A. and Ng, S.W. (2008) N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate. Acta Crystallographica Section E: Structure Reports Online, 64 (Pt 8). o1452. ISSN 1600-5368 http://www.ncbi.nlm.nih.gov/pubmed/21203167 21203167
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
topic QD Chemistry
spellingShingle QD Chemistry
Yehye, W.A.
Ariffin, A.
Ng, S.W.
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
description The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the other Schiff base mol-ecule, the 2-hydr-oxy-substituted benzene ring is oriented so that the 2-hydr-oxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base mol-ecules inter-act with methanol solvent to furnish a hydrogen-bonded chain.
format Article
author Yehye, W.A.
Ariffin, A.
Ng, S.W.
author_facet Yehye, W.A.
Ariffin, A.
Ng, S.W.
author_sort Yehye, W.A.
title N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
title_short N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
title_full N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
title_fullStr N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
title_full_unstemmed N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
title_sort n'-(3,5-di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
publisher International Union of Crystallography
publishDate 2008
url http://eprints.um.edu.my/924/
http://www.ncbi.nlm.nih.gov/pubmed/21203167
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score 13.209306

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