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N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate

The asymmetric unit of the title compound, C22H28N2O3 center dot CH4O, consists of two independent Schiff base molecules and two independent methanol solvent molecules. In one Schiff base molecule, the 2-hydroxy group forms an intramolecular hydrogen bond with the amide O atom, whereas in the other...

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Main Authors: Ariffin, Azhar, Ng, S.W., Yehye, W.A.
Format: Article
Language:English
Published: International Union of Crystallography 2008
Subjects:
QD Chemistry
Online Access:http://eprints.um.edu.my/8071/1/Yehye-2008-N%27-%283%2C5-Di-tert-buty.pdf
http://eprints.um.edu.my/8071/
http://journals.iucr.org/e/issues/2008/08/00/lh2656/lh2656.pdf
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spelling my.um.eprints.80712019-01-31T01:00:57Z http://eprints.um.edu.my/8071/ N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate Ariffin, Azhar Ng, S.W. Yehye, W.A. QD Chemistry The asymmetric unit of the title compound, C22H28N2O3 center dot CH4O, consists of two independent Schiff base molecules and two independent methanol solvent molecules. In one Schiff base molecule, the 2-hydroxy group forms an intramolecular hydrogen bond with the amide O atom, whereas in the other Schiff base molecule, the 2-hydroxy-substituted benzene ring is oriented so that the 2-hydroxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base molecules interact with methanol solvent to furnish a hydrogen-bonded chain. International Union of Crystallography 2008 Article PeerReviewed application/pdf en http://eprints.um.edu.my/8071/1/Yehye-2008-N%27-%283%2C5-Di-tert-buty.pdf Ariffin, Azhar and Ng, S.W. and Yehye, W.A. (2008) N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate. Acta Crystallographica Section E: Structure Reports Online, 64 (8). O1452-U1931. ISSN 1600-5368 http://journals.iucr.org/e/issues/2008/08/00/lh2656/lh2656.pdf 10.1107/s1600536808020746
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Ariffin, Azhar
Ng, S.W.
Yehye, W.A.
N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
description The asymmetric unit of the title compound, C22H28N2O3 center dot CH4O, consists of two independent Schiff base molecules and two independent methanol solvent molecules. In one Schiff base molecule, the 2-hydroxy group forms an intramolecular hydrogen bond with the amide O atom, whereas in the other Schiff base molecule, the 2-hydroxy-substituted benzene ring is oriented so that the 2-hydroxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base molecules interact with methanol solvent to furnish a hydrogen-bonded chain.
format Article
author Ariffin, Azhar
Ng, S.W.
Yehye, W.A.
author_facet Ariffin, Azhar
Ng, S.W.
Yehye, W.A.
author_sort Ariffin, Azhar
title N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
title_short N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
title_full N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
title_fullStr N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
title_full_unstemmed N'-(3,5-Di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
title_sort n'-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-hydroxybenzohydrazide methanol solvate
publisher International Union of Crystallography
publishDate 2008
url http://eprints.um.edu.my/8071/1/Yehye-2008-N%27-%283%2C5-Di-tert-buty.pdf
http://eprints.um.edu.my/8071/
http://journals.iucr.org/e/issues/2008/08/00/lh2656/lh2656.pdf
_version_ 1643688210336841728
score 13.209306

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