Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system

Purpose - The purpose of this paper is to evaluate the stability of anthocyanin colorant with and without ferulic acid (FA) stabilising agent in a polyvinyl alcohol (PVA) binder coating system. Design/methodology/approach - The anthocyanin colorant was extracted using methanol acidified with 0.5 tri...

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Main Authors: Aziz, N., Nor, N.A.M., Mohd-Adnan, A.F., Taha, R.M., Arof, Abdul Kariem
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Published: Emerald 2012
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Online Access:http://eprints.um.edu.my/10773/
https://doi.org/10.1108/03699421211242455
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spelling my.um.eprints.107732018-10-04T08:56:34Z http://eprints.um.edu.my/10773/ Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system Aziz, N. Nor, N.A.M. Mohd-Adnan, A.F. Taha, R.M. Arof, Abdul Kariem QH301 Biology Purpose - The purpose of this paper is to evaluate the stability of anthocyanin colorant with and without ferulic acid (FA) stabilising agent in a polyvinyl alcohol (PVA) binder coating system. Design/methodology/approach - The anthocyanin colorant was extracted using methanol acidified with 0.5 trifluoroacetic acid (TEA). FA was added to improve thermal stability of the colorant. The FA added colorant was mixed with PVA to develop a coating system. To test the ability of the coating mixture to withstand heat in the liquid state, spectroscopic studies were carried out in the visible region of the electromagnetic spectrum when the liquid samples had cooled down to room temperature after being heated at 80 and 90 degrees C for 30 minutes. This procedure was repeated six times until a total heating time of 180 minutes has been accomplished. The liquid samples were also coated on glass slides, cured and then stored in different incubators at 30, 40 and 50 degrees C. The visible spectrum was taken everyday for 30 days to study the effect of storage temperature. Spectroscopic results were analysed in terms of intensity rate percentage (IRP). Findings - In the liquid state, the anthocyanin-PVA mixture without FA showed lower absorbance compared to the mixture containing FA after heating at 80 and 90 degrees C. This shows that FA can enhance the intensity of absorbance of the liquid coating mixture. The mixtures containing FA show increase in absorbance with increase in heating time. The same results are obtained for the coating on glass substrate where FA containing coatings show increase in IRP with time for all storage temperatures. Coating with 1 FA content showed better enhancement and stability. Research limitations/implications - The colour of the untreated samples quickly faded during heating and storage at different temperatures. In this study, the addition of 0.5 and 1 FA stabilised and enhanced the colour intensity at 30, 40 and 50 degrees C. Further improvements may find the mixture suitable as paint or coating materials and as nail varnish. Practical implications - The results indicate the possibility of applying the FA stabilised anthocyanin-PVA, colorant-binder composition in a coating system. Originality/value - The use of anthocyanin from M. Malabathricum as a colourant in a coating system or nail varnish is original. Anthocyanin pigments are normally used as colorant in foods. Emerald 2012 Article PeerReviewed Aziz, N. and Nor, N.A.M. and Mohd-Adnan, A.F. and Taha, R.M. and Arof, Abdul Kariem (2012) Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system. Pigment & Resin Technology, 41 (4). pp. 223-229. ISSN 0369-9420 https://doi.org/10.1108/03699421211242455 doi:10.1108/03699421211242455
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
topic QH301 Biology
spellingShingle QH301 Biology
Aziz, N.
Nor, N.A.M.
Mohd-Adnan, A.F.
Taha, R.M.
Arof, Abdul Kariem
Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
description Purpose - The purpose of this paper is to evaluate the stability of anthocyanin colorant with and without ferulic acid (FA) stabilising agent in a polyvinyl alcohol (PVA) binder coating system. Design/methodology/approach - The anthocyanin colorant was extracted using methanol acidified with 0.5 trifluoroacetic acid (TEA). FA was added to improve thermal stability of the colorant. The FA added colorant was mixed with PVA to develop a coating system. To test the ability of the coating mixture to withstand heat in the liquid state, spectroscopic studies were carried out in the visible region of the electromagnetic spectrum when the liquid samples had cooled down to room temperature after being heated at 80 and 90 degrees C for 30 minutes. This procedure was repeated six times until a total heating time of 180 minutes has been accomplished. The liquid samples were also coated on glass slides, cured and then stored in different incubators at 30, 40 and 50 degrees C. The visible spectrum was taken everyday for 30 days to study the effect of storage temperature. Spectroscopic results were analysed in terms of intensity rate percentage (IRP). Findings - In the liquid state, the anthocyanin-PVA mixture without FA showed lower absorbance compared to the mixture containing FA after heating at 80 and 90 degrees C. This shows that FA can enhance the intensity of absorbance of the liquid coating mixture. The mixtures containing FA show increase in absorbance with increase in heating time. The same results are obtained for the coating on glass substrate where FA containing coatings show increase in IRP with time for all storage temperatures. Coating with 1 FA content showed better enhancement and stability. Research limitations/implications - The colour of the untreated samples quickly faded during heating and storage at different temperatures. In this study, the addition of 0.5 and 1 FA stabilised and enhanced the colour intensity at 30, 40 and 50 degrees C. Further improvements may find the mixture suitable as paint or coating materials and as nail varnish. Practical implications - The results indicate the possibility of applying the FA stabilised anthocyanin-PVA, colorant-binder composition in a coating system. Originality/value - The use of anthocyanin from M. Malabathricum as a colourant in a coating system or nail varnish is original. Anthocyanin pigments are normally used as colorant in foods.
format Article
author Aziz, N.
Nor, N.A.M.
Mohd-Adnan, A.F.
Taha, R.M.
Arof, Abdul Kariem
author_facet Aziz, N.
Nor, N.A.M.
Mohd-Adnan, A.F.
Taha, R.M.
Arof, Abdul Kariem
author_sort Aziz, N.
title Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
title_short Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
title_full Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
title_fullStr Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
title_full_unstemmed Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system
title_sort study of anthocyanin stability derived from the fruit pulp of melastoma malabathricum in a coating system
publisher Emerald
publishDate 2012
url http://eprints.um.edu.my/10773/
https://doi.org/10.1108/03699421211242455
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score 13.160551