Effects of drying temperature and solvent concentration on the separation properties of polyamide 6 membrane / Kamil, R.N.M …[et al.]

The effects of drying temperature and solvent concentration on the separation properties of polyamide 6 membrane were investigated In this study, polyamide 6 membranes were prepared by casting 10-20 wt% solution of polymer in 85 wt% formic acid onto a glass plate and precipitation in water. The memb...

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Bibliographic Details
Main Authors: Kamil, R.N.M, F., Shamsuddin, Z., Man, N.Y, Yuhana
Format: Conference or Workshop Item
Language:English
Published: 2006
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/81655/1/81655.PDF
https://ir.uitm.edu.my/id/eprint/81655/
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Summary:The effects of drying temperature and solvent concentration on the separation properties of polyamide 6 membrane were investigated In this study, polyamide 6 membranes were prepared by casting 10-20 wt% solution of polymer in 85 wt% formic acid onto a glass plate and precipitation in water. The membranes prepared were dried for 1 hour at different temperatures ranging from 40 to 130°C The separation properties of the membranes were studied with binary water-ethanol mixtures consisting of 40 wt% ethanol. The drying temperature as well as the solvent concentration of PA 6 solution influenced the separation properties of PA 6 membrane. The separation of ethanol from water was optimum using membrane which was dried at 70°C However, as the drying temperature increased, the extraction of ethanol decreased due to reduction in pore size. Similarly, as the solvent concentration decreased, the ethanol separation also decreased as a result of smaller pore size. These effects were confirmed by SEM micrographs.