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The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli

Nanastructured porous silicon template (NPSiT) was successfully prepared from [100] orientation p-doped silicon (Si) substrate by photo-electrochemically anodization method with optimization parameters of etching time and annealing temperature while the rest of parameters were fixed. Uniform porous...

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Main Author: Asli, Noor Asnida
Format: Book Section
Language:English
Published: Institute of Graduate Studies, UiTM 2015
Subjects:
Malaysia
Online Access:http://ir.uitm.edu.my/id/eprint/19271/1/ABS_NOOR%20ASNIDA%20ASLI%20TDRA%20VOL%207%20IGS%2015.pdf
http://ir.uitm.edu.my/id/eprint/19271/
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spelling my.uitm.ir.192712018-06-12T07:27:57Z http://ir.uitm.edu.my/id/eprint/19271/ The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli Asli, Noor Asnida Malaysia Nanastructured porous silicon template (NPSiT) was successfully prepared from [100] orientation p-doped silicon (Si) substrate by photo-electrochemically anodization method with optimization parameters of etching time and annealing temperature while the rest of parameters were fixed. Uniform porous structures, optimum surface roughness and high intensity of photoluminescence (PL) of NPSiT as an optimized samples. The optimized NPSiT was used as template to synthesis vertically aligned carbon nanotubes (VACNT). VACNT were synthesized on NPSiT using double thermal chemical vapour deposition (DTCVD) method with camphor oil as carbon source and ferrocene (Fe) as a catalyst. The synthesis was carried out by the in-situ catalyst with floated method in a DTCVD reactor without any pre-treatment of catalyst. The process was called in-situ catalyst due to same vaporization point, 180°C of camphor and ferrocene. High percentage of vertically aligned, smallest diameter, uniform length, high graphite crystallinity and high growth rate of VACNT on NPSiT has been successfully synthesized with short synthesis time at 15 min. Single-Walled Carbon Nanotubes (SWCNT) was found at 15 min synthesis time gave lowest ID/IG ratio. Parametric studies were done such as ratio of catalyst to carbon source, synthesis temperature and synthesis time to determine optimum parameter in obtain VACNT on NPSiT… Institute of Graduate Studies, UiTM 2015 Book Section PeerReviewed text en http://ir.uitm.edu.my/id/eprint/19271/1/ABS_NOOR%20ASNIDA%20ASLI%20TDRA%20VOL%207%20IGS%2015.pdf Asli, Noor Asnida (2015) The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli. In: The Doctoral Research Abstracts. IPSis Biannual Publication, 7 (7). Institute of Graduate Studies, UiTM, Shah Alam.
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Malaysia
spellingShingle Malaysia
Asli, Noor Asnida
The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
description Nanastructured porous silicon template (NPSiT) was successfully prepared from [100] orientation p-doped silicon (Si) substrate by photo-electrochemically anodization method with optimization parameters of etching time and annealing temperature while the rest of parameters were fixed. Uniform porous structures, optimum surface roughness and high intensity of photoluminescence (PL) of NPSiT as an optimized samples. The optimized NPSiT was used as template to synthesis vertically aligned carbon nanotubes (VACNT). VACNT were synthesized on NPSiT using double thermal chemical vapour deposition (DTCVD) method with camphor oil as carbon source and ferrocene (Fe) as a catalyst. The synthesis was carried out by the in-situ catalyst with floated method in a DTCVD reactor without any pre-treatment of catalyst. The process was called in-situ catalyst due to same vaporization point, 180°C of camphor and ferrocene. High percentage of vertically aligned, smallest diameter, uniform length, high graphite crystallinity and high growth rate of VACNT on NPSiT has been successfully synthesized with short synthesis time at 15 min. Single-Walled Carbon Nanotubes (SWCNT) was found at 15 min synthesis time gave lowest ID/IG ratio. Parametric studies were done such as ratio of catalyst to carbon source, synthesis temperature and synthesis time to determine optimum parameter in obtain VACNT on NPSiT…
format Book Section
author Asli, Noor Asnida
author_facet Asli, Noor Asnida
author_sort Asli, Noor Asnida
title The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
title_short The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
title_full The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
title_fullStr The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
title_full_unstemmed The synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / Noor Asnida Asli
title_sort synthesis of vertically aligned carbon nanotubes on nanostructured porous silicon template by in-situ catalyst double thermal chemical vapour deposition method / noor asnida asli
publisher Institute of Graduate Studies, UiTM
publishDate 2015
url http://ir.uitm.edu.my/id/eprint/19271/1/ABS_NOOR%20ASNIDA%20ASLI%20TDRA%20VOL%207%20IGS%2015.pdf
http://ir.uitm.edu.my/id/eprint/19271/
_version_ 1685649190634389504
score 13.160551

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