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Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin

A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80...

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Main Authors: Che Soh, Siti Kamilah, Jusoh, Siti Aminah, Shamsuddin, Mustaffa
Format: Article
Language:English
Published: Research Management Institute (RMI) 2014
Subjects:
Palladium
Polystyrene
Online Access:http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf
http://ir.uitm.edu.my/id/eprint/12430/
https://srj.uitm.edu.my/
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spelling my.uitm.ir.124302016-05-26T02:46:51Z http://ir.uitm.edu.my/id/eprint/12430/ Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Palladium Polystyrene A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. Research Management Institute (RMI) 2014 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf Che Soh, Siti Kamilah and Jusoh, Siti Aminah and Shamsuddin, Mustaffa (2014) Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin. Scientific Research Journal, 11 (2). pp. 1-10. ISSN 1675-7009 https://srj.uitm.edu.my/
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Palladium
Polystyrene
spellingShingle Palladium
Polystyrene
Che Soh, Siti Kamilah
Jusoh, Siti Aminah
Shamsuddin, Mustaffa
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
description A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy.
format Article
author Che Soh, Siti Kamilah
Jusoh, Siti Aminah
Shamsuddin, Mustaffa
author_facet Che Soh, Siti Kamilah
Jusoh, Siti Aminah
Shamsuddin, Mustaffa
author_sort Che Soh, Siti Kamilah
title Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_short Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_full Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_fullStr Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_full_unstemmed Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_sort synthesis and physicochemical analysis of polystyrene-anchored pd(ii) metal complex / siti kamilah che soh, siti aminah jusoh and mustaffa shamsuddin
publisher Research Management Institute (RMI)
publishDate 2014
url http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf
http://ir.uitm.edu.my/id/eprint/12430/
https://srj.uitm.edu.my/
_version_ 1685648366552219648
score 13.154949

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