Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80...
Saved in:
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Research Management Institute (RMI)
2014
|
Subjects: | |
Online Access: | http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf http://ir.uitm.edu.my/id/eprint/12430/ https://srj.uitm.edu.my/ |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
id |
my.uitm.ir.12430 |
---|---|
record_format |
eprints |
spelling |
my.uitm.ir.124302016-05-26T02:46:51Z http://ir.uitm.edu.my/id/eprint/12430/ Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Palladium Polystyrene A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. Research Management Institute (RMI) 2014 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf Che Soh, Siti Kamilah and Jusoh, Siti Aminah and Shamsuddin, Mustaffa (2014) Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin. Scientific Research Journal, 11 (2). pp. 1-10. ISSN 1675-7009 https://srj.uitm.edu.my/ |
institution |
Universiti Teknologi Mara |
building |
Tun Abdul Razak Library |
collection |
Institutional Repository |
continent |
Asia |
country |
Malaysia |
content_provider |
Universiti Teknologi Mara |
content_source |
UiTM Institutional Repository |
url_provider |
http://ir.uitm.edu.my/ |
language |
English |
topic |
Palladium Polystyrene |
spellingShingle |
Palladium Polystyrene Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
description |
A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The
properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. |
format |
Article |
author |
Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa |
author_facet |
Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa |
author_sort |
Che Soh, Siti Kamilah |
title |
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
title_short |
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
title_full |
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
title_fullStr |
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
title_full_unstemmed |
Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
title_sort |
synthesis and physicochemical analysis of polystyrene-anchored pd(ii) metal complex / siti kamilah che soh, siti aminah jusoh and mustaffa shamsuddin |
publisher |
Research Management Institute (RMI) |
publishDate |
2014 |
url |
http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf http://ir.uitm.edu.my/id/eprint/12430/ https://srj.uitm.edu.my/ |
_version_ |
1685648366552219648 |
score |
13.18916 |