Crystal structure of [meso-5,7,7,12,14,14,-hexamethyl-1,4,8,11-tetraazacyclotetradecane]nickel(II) diperchlorate – dimethylsulphoxide (1/2), C20H48Cl2N4NiO10S2

• Main Authors: Rabi, S., Dey, L., Palit, D., Dey, B. K., Rahman, Ismail M. M., Tiekink, Edward R. T. *, Roy, T. G.
• Format: Article
• Language: English
• Published: De Gruyter Open 2021
• Subjects: QD Chemistry
• Online Access: http://eprints.sunway.edu.my/1971/1/Tiekink%20ZK_NCS%202021_1243.pdf; http://eprints.sunway.edu.my/1971/; http://doi.org/10.1515/ncrs-2021-0291

C20H48Cl2N4NiO10S2, monoclinic, P21/n (no. 14), a = 8.657(2) Å, b = 15.233(4) Å, c = 11.956(3) Å, β = 102.737(2)°, V = 1537.9(7) Å3, Z = 2, R gt (F) = 0.0237, wR ref (F 2) = 0.0655, T = 93(2) K.